苯并[b]噻吩-2(3H)-酮合成路线 （共 15 条）
反应条件
dihydrogen peroxide in water
T=20°C; 8 h;
参考文献
Chen, Shuyi; Zhao, Xianrui; Chen, Jingyi; Chen, Jin; Kuznetsova, Larisa; Wong, Stanislaus S.; Ojima, Iwao
Bioconjugate Chemistry, 2010 , vol. 21, # 5 p. 979 - 987
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-20 - 20°C;
参考文献
Kamila, Sukanta; Biehl, Edward R.
Heterocycles, 2004 , vol. 63, # 8 p. 1813 - 1819
反应条件
1: With tetra-n-butylammonium perchlorate; oxygen in acetonitrile
T=20°C; Electrolysis;
2: With sulfuric acid; water in acetonitrile
参考文献
Hosoi, Kohei; Kuriyama, Yu; Inagi, Shinsuke; Fuchigami, Toshio
Chemical Communications, 2010 , vol. 46, # 8 p. 1284 - 1286
反应条件
formic acid
1 h; Heating;
参考文献
Watanabe; Date; Kawanishi; Akiyoshi; Furukawa
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 1 p. 173 - 176
反应条件
1.1: NaH / tetrahydrofuran / 1 h / 20 °C
1.2: tetrahydrofuran / 0 °C
2.1: 78 percent / diisopropylamine; BuLi / tetrahydrofuran; hexane / -20 - 20 °C
View Scheme
参考文献
Kamila, Sukanta; Biehl, Edward R.
Heterocycles, 2004 , vol. 63, # 8 p. 1813 - 1819
反应条件
Equilibrium constant;
参考文献
Capon, Brian; Kwok, Fu-Chiu; Road, Pokfulam
Tetrahedron Letters, 1986 , vol. 27, # 28 p. 3275 - 3278
反应条件
potassium hydroxide; ethanol
T=200°C;
参考文献
Komppa; Weckman
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 138, p. 109,116
反应条件
ethanol; hydrazine hydrate
Erhitzen der entstandenen Verbindung ueber ihren Schmelzpunkt;
参考文献
Marschalk
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. <2> 88, p. 246
参考文献
Marschalk
Chemische Berichte, 1912 , vol. 45, p. 1484
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. <2> 88, p. 239
参考文献
Komppa; Weckman
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 138, p. 109,116
Full Text Show Details
Glauert; Mann
Journal of the Chemical Society, 1952 , p. 2127,2131
