1-溴-2-(4-溴苯基)苯合成路线 （共 14 条）
反应条件
bromine; bis-[(trifluoroacetoxy)iodo]benzene in chloroform
Ambient temperature;
参考文献
Gallos, John; Varvoglis, Anastasios
Journal of Chemical Research, Miniprint, 1982 , # 6 p. 1649 - 1660
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=20°C; 1 h;
参考文献
Okano, Masateru; Amano, Masayuki; Takagi, Kentaro
Tetrahedron Letters, 1998 , vol. 39, # 19 p. 3001 - 3004
反应条件
1: FeCl3; water; bromine / 20 °C
2: tin (II)-chloride; ethanol
3: ueber die Diazonium-Verbindung
View Scheme
参考文献
Case
Journal of the American Chemical Society, 1938 , vol. 60, p. 424,426
反应条件
1: tin (II)-chloride; ethanol
2: ueber die Diazonium-Verbindung
View Scheme
参考文献
Case
Journal of the American Chemical Society, 1938 , vol. 60, p. 424,426
反应条件
Tl(OCOCF3)3; palladium diacetate
T=70°C; 60 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yatsimirsky, Anatoly K.; Deiko, Sergei A.; Ryabov, Alexander D.
Tetrahedron, 1983 , vol. 39, # 14 p. 2381 - 2392
反应条件
Tl(OCOCF3)3; palladium diacetate
T=70°C; 60 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Yatsimirsky, Anatoly K.; Deiko, Sergei A.; Ryabov, Alexander D.
Tetrahedron, 1983 , vol. 39, # 14 p. 2381 - 2392
反应条件
Tl(OCOCF3)3; palladium diacetate
T=70°C; 60 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yatsimirsky, Anatoly K.; Deiko, Sergei A.; Ryabov, Alexander D.
Tetrahedron, 1983 , vol. 39, # 14 p. 2381 - 2392
反应条件
ueber die Diazonium-Verbindung;
参考文献
Case
Journal of the American Chemical Society, 1938 , vol. 60, p. 424,426
反应条件
sulfuric acid
Diazotization.Behandlung der Diazoniumsalz-Loesung mit Hg(NO3)2 und KBr und Erhitzen des gebildeten Diazonium-tetrabromomercurats(II) mit KBr bis auf 120grad;
参考文献
Finzi; Bellavita
Gazzetta Chimica Italiana, 1934 , vol. 64, p. 335,343,
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 77,86
反应条件
1: tin; aqueous hydrochloric acid; ethanol
2: aqueous H2SO4 / Diazotization.Behandlung der Diazoniumsalz-Loesung mit wss. H3PO2
View Scheme
参考文献
Finzi; Bellavita
Gazzetta Chimica Italiana, 1934 , vol. 64, p. 335,343,
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 77,86
