1-(3-氨基-1-苯并呋喃-2-基)乙酮合成路线 (共 12 条)
反应条件
potassium carbonate in butanone T=82°C; 1 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 4 p. 625 - 635
反应条件
potassium carbonate in acetone 4 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 5 p. 391 - 393
反应条件
potassium carbonate in acetone 8 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 5 p. 391 - 393
反应条件
1: 59 percent / K2CO3 / acetone / 4 h / Heating 2: 93 percent / K2CO3 / acetone / 4 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 5 p. 391 - 393
反应条件
potassium hydroxide; hydroxylamine hydrochloride in ethanol
4 h; Heating;
参考文献
Gatta, Franco; Settimj, Guido
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1251 - 1254
反应条件
1: 79 percent / NH2OH.HCl, KOH / aq. ethanol / 4 h / Heating
2: 56 percent / pyridine / dioxane / 3 h / Ambient temperature
View Scheme
参考文献
Gatta, Franco; Settimj, Guido
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1251 - 1254
反应条件
1: 79 percent / NH2OH.HCl, KOH / aq. ethanol / 4 h / Heating
2: 1) pyridine, 2) 2N-NaOH / 1) dioxane, r.t., 3 h, 2) ethanol, r.t., 3 h
View Scheme
参考文献
Gatta, Franco; Settimj, Guido
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1251 - 1254
反应条件
1: 79 percent / NH2OH.HCl, KOH / aq. ethanol / 4 h / Heating
2: 1) pyridine, 2) 2N-NaOH / 1) dioxane, r.t., 3 h, 2) ethanol, r.t., 3 h
3: 86 percent / PCl3 / CHCl3 / 2 h / Heating
View Scheme
参考文献
Gatta, Franco; Settimj, Guido
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1251 - 1254
反应条件
pyridine in benzene
2 h; Ambient temperature;
参考文献
Gatta, Franco; Settimj, Guido
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1251 - 1254
反应条件
1: 89 percent / pyridine / benzene / 2 h / Ambient temperature
2: 1) NaH / 1) DMF, r.t., 1 h, 2) r.t., 2 h
View Scheme
参考文献
Gatta, Franco; Settimj, Guido
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1251 - 1254