[bis(acetoxy)iodo]benzene T=20°C; 2 h;

[bis(acetoxy)iodo]benzene

1: (i) TsCl, Py, (ii) /BRN= 1940395/ 2: (i) H2, Pd-C, AcOH, (ii) NaNO2, H2SO4, (iii) I2, aq. NaI, urea, CHCl3 3: aq. HI / acetic acid / Heating 4: B2H6 / tetrahydrofuran View Scheme

1: (i) TsCl, Py, (ii) /BRN= 1940395/ 2: (i) H2, Pd-C, AcOH, (ii) NaNO2, H2SO4, (iii) I2, aq. NaI, urea, CHCl3 3: aq. NaOH / Heating 4: B2H6 / tetrahydrofuran View Scheme