4,5-双(甲硫代)-1,3-二硫杂环戊烯-2-硫酮合成路线 （共 25 条）
反应条件
1) electrolysis; working electrode: platina foil, reference electrode: saturated calomel, counter electrode: carbon rod; electrolyte: 0.4 M TBAI in DMF; current: 0.2 A; potential: - 1.8 - -2.1 V; 2) warming 1 h; Yield given. Multistep reaction;
参考文献
Falsig, Mogens; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 591 - 596
反应条件
1) K 1) DMF, -5 - 0 deg C, 2) MeOH; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hartke, Klaus; Kissel, Thomas; Quante, Josef; Matusch, Rudolf
Chemische Berichte, 1980 , vol. 113, # 5 p. 1898 - 1906
反应条件
in acetonitrile Ambient temperature;
参考文献
Moltzen, Ejner Knud; Senning, Alexander; Hazell, Rita Gronbaek; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 7 p. 593 - 597
参考文献
Dyer, C. D.; Kilburn, J. D.; Maddams, W. F.; Walker, P. A.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1991 , vol. 47, # 9 p. 1225 - 1234
反应条件
T=80°C; P=3000240 Torr; 6 h; trimethyl phosphite; different pressure; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 3358 - 3359
反应条件
phosphorous acid trimethyl ester in benzene 4 h; Heating;
参考文献
Molecular Crystals and Liquid Crystals (1969-1991), , vol. 156, p. 269 - 276
反应条件
triethyl phosphite T=75 - 80°C; 2 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 19 p. 1408 - 1409
反应条件
triethyl phosphite T=90°C; 2 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 135, # 29 p. 10852 - 10862
反应条件
triethyl phosphite T=110°C; 30 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 4 p. 1343 - 1344
反应条件
triethyl phosphite T=120°C; 1 h;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 42, # 8 p. 1050 - 1051
