1-甲基-1,2,3,4-四氢异喹啉合成路线 （共 44 条）
反应条件
[CpIrI2]2 in toluene T=40°C;
参考文献
Tetrahedron Letters, , vol. 48, # 7 p. 1247 - 1250
反应条件
1: 1) tBuLi/TMEDA / 1) THF, -80 deg C, 5min 2: 77 percent / Na<AlH2(OCH2CH2OCH3)2> / benzene View Scheme
参考文献
Angewandte Chemie, , vol. 93, # 1 p. 125 - 126
反应条件
hydrazine hydrate; acetic acid in ethanol T=60°C;
参考文献
Synthetic Communications, , vol. 36, # 22 p. 3339 - 3343
反应条件
1: 36 percent / P2O5; POCl3 / toluene / Heating 2: 87 percent / NaBH4 / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 17 p. 2853 - 2855
反应条件
boron trifluoride diethyl etherate
参考文献
Heer, Jag P.; Harling, John D.; Thompson, Mervyn
Synthetic Communications, 2002 , vol. 32, # 16 p. 2555 - 2563
反应条件
1: 77 percent / pyridine / CH2Cl2 2: 36 percent / P2O5; POCl3 / toluene / Heating 3: 87 percent / NaBH4 / ethanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 17 p. 2853 - 2855
反应条件
C21H21ClIrNO2 in 2,2,2-trifluoroethanol 3 h; RefluxInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., , vol. 125, # 27 p. 7121 - 7125,5
