(2E,4E)-5-(4-氯苯基)-2,4-戊二烯醛合成路线 （共 8 条）
反应条件
aluminum oxide; potassium fluoride in tetrahydrofuran; diethyl ether; water
T=40°C; 30 h;
参考文献
Peng, Zhi-Hui; Li, Yun-Long; Wu, Wen-Lian; Liu, Cui-Xian; Wu, Yu-Lin
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 10 p. 1057 - 1066
反应条件
barium dihydroxide in tetrahydrofuran
Condensation; Cross aldol condensation; 4 h; Heating;
参考文献
Mahata; Barun; Ila; Junjappa
Synlett, 2000 , # 9 p. 1345 - 1347
反应条件
phosphoric acid; hydroquinone in 1,4-dioxane; water
T=100°C; 14 h; Yield given;
参考文献
Unterhalt; Eljabour; Milsmann
Archiv der Pharmazie, 1986 , vol. 319, # 12 p. 1130 - 1134
参考文献
Parameswara Reddy, M.; Krishna Rao, G. S.
Synthesis, 1980 , # 10 p. 815 - 818
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; Oxidation; 0.5 h;
参考文献
Oida, Sadao; Tajima, Yawara; Konosu, Toshiyuki; Nakamura, Yoshie; Somada, Atsushi; Tanaka, Teruo; Habuki, Shinobu; Harasaki, Tamako; Kamai, Yasuki; Fukuoka, Takashi; Ohya, Satoshi; Yasuda, Hiroshi
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 5 p. 694 - 707
反应条件
1: 80 percent / Ba(OH)2 / tetrahydrofuran / 6 h / Heating
2: 62 percent / Ba(OH)2 / tetrahydrofuran / 4 h / Heating
View Scheme
参考文献
Mahata; Barun; Ila; Junjappa
Synlett, 2000 , # 9 p. 1345 - 1347
反应条件
1: DIBAL / toluene / 0.75 h / 0 °C
2: MnO2 / CH2Cl2 / 0.5 h / 20 °C
View Scheme
参考文献
Oida, Sadao; Tajima, Yawara; Konosu, Toshiyuki; Nakamura, Yoshie; Somada, Atsushi; Tanaka, Teruo; Habuki, Shinobu; Harasaki, Tamako; Kamai, Yasuki; Fukuoka, Takashi; Ohya, Satoshi; Yasuda, Hiroshi
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 5 p. 694 - 707
反应条件
1: 92 percent / potassium borohydride / methanol / 2 h / 20 °C
2: POCl3
View Scheme
参考文献
Shi, De Qing; Chen, Ru Yu
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 229 - 237
