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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7-溴-D-色氨酸
合成路线
（共 9 条）
496929-98-7
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
hydrogen bromide T=100°C; 3 h;
参考文献
Konda-Yamada, Yaeko; Okada, Chiharu; Yoshida, Kiminari; Umeda, Yasuyuki; Arima, Shiho; Sato, Noriko; Kai, Toshitsugu; Takayanagi, Hiroaki; Harigaya, Yoshihiro
Tetrahedron, 2002 , vol. 58, # 39 p. 7851 - 7861
75816-18-1
→
反应条件
496929-99-8
7-溴-D-色氨酸
+
496930-04-2
反应条件
D-aminoacylase; cobalt(II) chloride in phosphate buffer T=37°C; pH=7.41; 24 h;
参考文献
Konda-Yamada, Yaeko; Okada, Chiharu; Yoshida, Kiminari; Umeda, Yasuyuki; Arima, Shiho; Sato, Noriko; Kai, Toshitsugu; Takayanagi, Hiroaki; Harigaya, Yoshihiro
Tetrahedron, 2002 , vol. 58, # 39 p. 7851 - 7861
51417-51-7
7-溴吲哚
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1: AcOH 2: D-aminoacylase; CoCl2*6H2O / aq. phosphate buffer / pH 7.4 View Scheme
参考文献
Yamada, Yaeko; Arima, Shiho; Okada, Chiharu; Akiba, Ai; Kai, Toshitsugu; Harigaya, Yoshihiro
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 6 p. 788 - 794
577-19-5
1-溴-2-硝基苯
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1: 53.8 percent / tetrahydrofuran / 0.33 h / -40 °C 2: 84.3 percent / acetic acid / 2 h / 75 °C 3: 42 percent / CoCl2*6H2O; L-aminoacylase / aq. phosphate buffer / 24 h / 37 °C / pH 7.41 4: 86.6 percent / aq. HBr / 3 h / 100 °C View Scheme
参考文献
Konda-Yamada, Yaeko; Okada, Chiharu; Yoshida, Kiminari; Umeda, Yasuyuki; Arima, Shiho; Sato, Noriko; Kai, Toshitsugu; Takayanagi, Hiroaki; Harigaya, Yoshihiro
Tetrahedron, 2002 , vol. 58, # 39 p. 7851 - 7861
75816-18-1
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1: 42 percent / CoCl2*6H2O; L-aminoacylase / aq. phosphate buffer / 24 h / 37 °C / pH 7.41 2: 86.6 percent / aq. HBr / 3 h / 100 °C View Scheme
参考文献
Konda-Yamada, Yaeko; Okada, Chiharu; Yoshida, Kiminari; Umeda, Yasuyuki; Arima, Shiho; Sato, Noriko; Kai, Toshitsugu; Takayanagi, Hiroaki; Harigaya, Yoshihiro
Tetrahedron, 2002 , vol. 58, # 39 p. 7851 - 7861
910808-42-3
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1: 94 percent / aq. NaOH / methanol / 0.5 h / 75 °C 2: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C 3: AcOH 4: D-aminoacylase; CoCl2*6H2O / aq. phosphate buffer / pH 7.4 View Scheme
参考文献
Yamada, Yaeko; Arima, Shiho; Okada, Chiharu; Akiba, Ai; Kai, Toshitsugu; Harigaya, Yoshihiro
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 6 p. 788 - 794
496-15-1
吲哚啉
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1.1: 94 percent / EDCI; pyridine / 24 h / 20 °C 2.1: trifluoroacetic acid; thallium trifluoroacetate / 11 h / 20 °C 2.2: 73 percent / CuBr2 / dimethylformamide / 2 h / 135 °C 3.1: 94 percent / aq. NaOH / methanol / 0.5 h / 75 °C 4.1: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C 5.1: AcOH 6.1: D-aminoacylase; CoCl2*6H2O / aq. phosphate buffer / pH 7.4 View Scheme
参考文献
Yamada, Yaeko; Arima, Shiho; Okada, Chiharu; Akiba, Ai; Kai, Toshitsugu; Harigaya, Yoshihiro
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 6 p. 788 - 794
2861-59-8
1-甲酸基吲哚啉
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1.1: trifluoroacetic acid; thallium trifluoroacetate / 11 h / 20 °C 1.2: 73 percent / CuBr2 / dimethylformamide / 2 h / 135 °C 2.1: 94 percent / aq. NaOH / methanol / 0.5 h / 75 °C 3.1: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C 4.1: AcOH 5.1: D-aminoacylase; CoCl2*6H2O / aq. phosphate buffer / pH 7.4 View Scheme
参考文献
Yamada, Yaeko; Arima, Shiho; Okada, Chiharu; Akiba, Ai; Kai, Toshitsugu; Harigaya, Yoshihiro
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 6 p. 788 - 794
62813-85-8
7-溴二氢吲哚
→
反应条件
496929-99-8
7-溴-D-色氨酸
反应条件
1: 73 percent / salcomine; O2 / methanol / 3 h / 20 °C 2: AcOH 3: D-aminoacylase; CoCl2*6H2O / aq. phosphate buffer / pH 7.4 View Scheme
参考文献
Yamada, Yaeko; Arima, Shiho; Okada, Chiharu; Akiba, Ai; Kai, Toshitsugu; Harigaya, Yoshihiro
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 6 p. 788 - 794
