thionyl chloride T=120°C; 0.833333 h;

1: 98 percent / SOCl2 / 0.83 h / 120 °C 2: 71 percent / AlCl3 / CH2Cl2 / 1.) -70 deg C, 1h; 2.) -60 deg C, 1h; 3.) -20 deg C, 1h View Scheme

1: 98 percent / SOCl2 / 0.83 h / 120 °C 2: 65 percent / AlCl3 / CH2Cl2 / 1.) -70 deg C, 1h; 2.) -40 deg C, 2h View Scheme

1: 98 percent / SOCl2 / 0.83 h / 120 °C 2: 17 percent / AlCl3 / CH2Cl2 / 1.) -70 deg C, 1h; 2.) -60 deg C, 1h; 3.) -20 deg C, 1h View Scheme

1: 98 percent / SOCl2 / 0.83 h / 120 °C 2: 71 percent / AlCl3 / CH2Cl2 / 1.) -70 deg C, 1h; 2.) -60 deg C, 1h; 3.) -20 deg C, 1h 3: 82 percent / HCl / CHCl3 / 20 h / Ambient temperature View Scheme