4’-甲基[1,1’-联苯]-4-甲酸甲酯合成路线 （共 47 条）
反应条件
NHC-Pd(II)-Im; tetrabutyl ammonium fluoride in toluene T=120°C; Hiyama reaction; 3 h; Inert atmosphere;
参考文献
Gu, Zheng-Song; Shao, Li-Xiong; Lu, Jian-Mei
Journal of Organometallic Chemistry, 2012 , vol. 700, p. 132 - 134
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in ethanol; water T=50°C; Suzuki-Miyaura Coupling; 5 h; Reagent/catalyst;
参考文献
Kuno, Shinichi; Kimura, Tomoyuki; Yamaguchi, Masanori
Tetrahedron Letters, 2014 , vol. 55, # 3 p. 720 - 724
反应条件
1: (4-methoxycarbonylphenyl)-boronic acid With iodine; potassium carbonate in acetonitrile T=80°C; 8 h; Inert atmosphereSchlenk techniqueSealed tube; 2: p-methylphenylboronic acid With palladium diacetate in acetonitrile T=80°C; Suzuki Coupling; 14 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Niu, Liting; Zhang, Hao; Yang, Haijun; Fu, Hua
Synlett, 2014 , vol. 25, # 7 art. no. 691, p. 995 - 1000
反应条件
potassium phosphate; PdCl2/4GLCAphos T=80°C; Substitution; 16 h;
参考文献
Nishimura, Masato; Ueda, Masato; Miyaura, Norio
Tetrahedron, 2002 , vol. 58, # 29 p. 5779 - 5787
反应条件
potassium phosphate; tris(dibenzylideneacetone)dipalladium (0) in toluene T=100°C; Suzuki-Miyaura coupling; 24 h;
参考文献
So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Organic Letters, 2007 , vol. 9, # 15 p. 2795 - 2798
反应条件
palladium diacetate in water; N,N-dimethyl-formamide T=20°C; 5 h;
参考文献
Yamamoto, Yasunori; Takizawa, Miho; Yu, Xiao-Qiang; Miyaura, Norio
Angewandte Chemie - International Edition, 2008 , vol. 47, # 5 p. 928 - 931
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water; tri-cyclo-hexyl-phosphine in 1,4-dioxane T=110°C; 12 h; Inert atmosphere;
参考文献
Guan, Bing-Tao; Wang, Yang; Li, Bi-Jie; Yu, Da-Gang; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14468 - 14470
反应条件
potassium phosphate; palladium diacetate in tert-butyl alcohol T=110°C; Suzuki-Miyaura coupling; 2 h;
参考文献
So, Chau Ming; Lau, Chak Po; Chan, Albert S. C.; Kwong, Fuk Yee
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7731 - 7734
反应条件
potassium phosphate; NiCl2(dppe); 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane T=110°C; Suzuki-Miyaura cross-coupling; 18 h; Inert atmosphere;
参考文献
Rosen, Brad M.; Huang, Chenghong; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 12 p. 2597 - 2600
反应条件
sodium hydroxide; Pd(NH3)2Cl2 in water T=120°C; Hiyama coupling; 3 h;
参考文献
Chen, Shao-Nung; Wu, Wei-Yi; Tsai, Fu-Yu
Tetrahedron, 2008 , vol. 64, # 35 p. 8164 - 8168
