RhH2(O2COH)(P(i-Pr)3)2 in tetrahydrofuran
T=120°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
1.1: NaH / tetrahydrofuran / 0.5 h / 25 °C
1.2: 49 percent / tetrahydrofuran / 14 h / 20 °C
2.1: NaH / tetrahydrofuran / 25 °C
2.2: 80 percent / tetrahydrofuran / 20 °C
View Scheme
参考文献
Curran, Dennis P.; Fairweather, Neil
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2972 - 2974
