反应条件
1: palladium diacetate; triphenylphosphine; potassium phosphate / tetrahydrofuran / 5.5 h / 20 °C / |Reflux; |Inert atmosphere 2: sodium hydroxide; water / methanol; tetrahydrofuran / 3 h / |Reflux 3: thionyl chloride / N,N-dimethyl-formamide; tetrahydrofuran / 1 h / 20 - 30 °C 4: triethylamine / N,N-dimethyl-formamide; tetrahydrofuran / 1.5 h / 45 - 55 °C View Scheme
参考文献
Ikemoto, Tomomi; Ito, Tatsuya; Nishiguchi, Atsuko; Miura, Syotaro; Tomimatsu, Kiminori
Organic Process Research and Development, 2005 , vol. 9, # 2 p. 168 - 173
