1,5-二氢苯并[b][1,4]二氮杂卓-2,4-二酮合成路线 （共 14 条）
反应条件
1: Darstellung
View Scheme
参考文献
Meyer,R.; Maier,J.
Justus Liebigs Annalen der Chemie, 1903 , vol. 327, p. 41
反应条件
hydrogenchloride; 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide
multistep reaction; other N-carboxy anhydrides; other Boc-anthranilic acid; synthesis 1,4-benzodiazepine-2,5-diones;
参考文献
Akssira; Kasmi; Dahdouh; Boumzebra
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1887 - 1888
反应条件
phosphorus pentachloride
1) 20 deg C, 23.5 h, 2) 4 h, 20 deg C; Yield given. Multistep reaction;
参考文献
Dolenz, Gerhard; Kollenz, Gert
Chemische Berichte, 1982 , vol. 115, # 2 p. 593 - 600
反应条件
1: 1) PCl5 / 1) 20 deg C, 23.5 h, 2) 4 h, 20 deg C
2: 80 percent / CrO3, glacial acetic acid, H2O / 1) 50 deg C, 40 min, 2) 12 h, 20 deg C
View Scheme
参考文献
Dolenz, Gerhard; Kollenz, Gert
Chemische Berichte, 1982 , vol. 115, # 2 p. 593 - 600
