4-羟基-3-甲氧基苄醇合成路线 （共 134 条）
反应条件
1: K2CO3 / ethanol 2: HCl / CH2Cl2 3: dimethylformamide View Scheme
参考文献
Andresen; Davis; Long
Journal of Pharmaceutical Sciences, 1979 , vol. 68, # 3 p. 283 - 288
反应条件
potassium carbonate in acetone Heating;
参考文献
Canceill,J.; Collet,A.; Gabard,J.
Journal of the American Chemical Society, 1985 , vol. 107, p. 1299
反应条件
potassium carbonate; caesium carbonate in dimethyl sulfoxide T=20°C; 15 h; Molecular sieveInert atmosphere;
参考文献
He; Ye; Mou; Chen; Li
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 8 p. 3345 - 3349
反应条件
in diethyl ether T=0°C;
参考文献
Phytochemistry (Elsevier), , vol. 37, # 4 p. 1165 - 1174
反应条件
1: 13.7 percent / 0.1 N KOH, 0.05 N LiClO4 / acetonitrile; H2O / 0 °C / anodic oxidation at Pt electrode 2: 87.6 percent / 0.1 N KOH, 0.05 N LiClO4 / acetonitrile; H2O / 0 °C / anodic oxidation at Pt electrode 3: 79.9 percent / 0.1 N KOH, 0.05 N LiClO4 / acetonitrile; H2O / 0 °C / cathodic reduction at Pt electrode View Scheme
参考文献
Yanilkin, V. V.; Dudenko, L. Yu.; Babkin, V. A.; Ivanova, S. Z.; Medvedev, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 5 p. 1139 - 1145,1001 - 1006
反应条件
RbF in acetonitrile T=80°C; 2 h;
参考文献
Miyazawa, Toshifumi; Yamamoto, Masato; Danjo, Hiroshi
Monatshefte fur Chemie, 2013 , vol. 144, # 9 p. 1351 - 1354
反应条件
pyridine 16.5 h; Ambient temperature;
参考文献
Nagao; Fujita; Kohno; Yagi
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 11 p. 3202 - 3207
反应条件
1: 1-butyl-3-methylimidazolium tetrachloroindate / 0.04 h / Microwave irradiation 2: 1-butyl-3-methylimidazolium tetrachloroindate / 0.05 h / 145 - 150 °C / Microwave irradiation View Scheme
参考文献
Mohammadpoor-Baltork; Moghadam; Tangestaninejad; Mirkhani; Khosropour; Mirjafari
Journal of the Iranian Chemical Society, 2011 , vol. 8, # 2 p. 513 - 524
反应条件
potassium carbonate in acetone T=80°C;
参考文献
Brotin, Thierry; Dutasta, Jean-Pierre
European Journal of Organic Chemistry, 2003 , # 6 p. 973 - 984
反应条件
sodium hydroxide in ethanol 3 h; Heating;
参考文献
Canceill, Josette; Collet, Andre
Journal of the Chemical Society, Chemical Communications, 1988 , p. 582 - 584
