4-羟基-3-甲氧基苄醇合成路线 (共 134 条)
反应条件
1.1: 27.3 g / p-TSA / methanol / 6 h / 20 °C 2.1: n-BuLi / tetrahydrofuran / 4.25 h / -15 - 0 °C 2.2: tetrahydrofuran; CH2Cl2 / -10 °C 3.1: 14.5 g / DDQ / CH2Cl2; H2O / 2 h / 20 °C View Scheme
参考文献
Cook, Silas P.; Christoph, Gaul; Danishefsky, Samuel J.
Tetrahedron Letters, 2005 , vol. 46, # 5 p. 843 - 847
反应条件
Novozym 435 T=50°C; 16 h; Polyacrylate;
参考文献
AJINOMOTO CO., INC.
Patent: WO2006/88239 A1, 2006 ;
Location in patent: Page/Page column 40-41 ;
反应条件
novozyme 435 T=25°C; 45 h;
参考文献
Sagawa, Koichiro; Takino, Yoshinobu; Amino, Yusuke
Patent: US2006/287390 A1, 2006 ;
Location in patent: Page/Page column 8 ;
反应条件
NaClO adsorbed on montmorillonite K10 in dichloromethane T=20°C; Oxidation; 0.416667 h;
参考文献
Layek, Keya; Maheswaran; Arundhathi; Kantam, M. Lakshmi; Bhargava, Suresh K.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 606 - 616
反应条件
oxygen; lt;bislt;(salicylideneamino)ethylgt;aminegt;cobalt in methanol P=2585.7 Torr; 17 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2398 - 2404
反应条件
potassium hydroxide; lithium perchlorate in water; acetonitrile T=0°C; anodic oxidation at Pt electrode;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 56, # 5 p. 1139 - 1145,1001 - 1006
反应条件
tricobalt tetroxide; oxygen in isopropyl alcohol T=80°C; P=5100.51 Torr; 6 h; Autoclave;
参考文献
Jha, Ajay; Rode, Chandrashekhar V.
New Journal of Chemistry, 2013 , vol. 37, # 9 p. 2669 - 2674
反应条件
Melanocarpus albomyces laccase; oxygen in 1,4-dioxane 24 h; sodium succinate buffer;
参考文献
Maarit, Lahtinen; Kristiina, Kruus; Petri, Heinonen; Jussi, Sipilae
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 18 p. 8357 - 8365
反应条件
dihydrogen peroxide; acetic acid; methyltrioxorhenium(VII) supported on poly(4-vinylpyridine) T=20°C; 6 h; Product distribution; Further Variations:Catalysts;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 15 p. 5292 - 5302
反应条件
silver(l) oxide in acetone Yield given. Yields of byproduct given;
参考文献
Ralph, John; Quideau, Stephane; Grabber, John H.; Haffield, Ronald D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 23 p. 3485 - 3498