4-羟基-3-甲氧基苄醇合成路线 （共 134 条）
反应条件
hydrogen in decalin T=250°C; P=37503.8 Torr; 20 h; Autoclave;
参考文献
Deutsch, Keenan L.; Shanks, Brent H.
Applied Catalysis A: General, 2012 , vol. 447-448, p. 144 - 150
反应条件
1: With TentaGel-N(R)C(O)CH2C2F4OC2F4SO2F; potassium carbonate in N,N-dimethyl-formamide T=20°C; 2: With formic acid; 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=85°C; 2 h; Further stages.;
参考文献
Pan, Yijun; Holmes, Christopher P.
Organic Letters, 2001 , vol. 3, # 17 p. 2769 - 2770
反应条件
sulfuric acid; nitric acid; HNO2 T=25°C; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 10 p. 1845 - 1850
Zhurnal Organicheskoi Khimii, , vol. 19, # 10 p. 2124 - 2130
反应条件
1: 60 percent / dimethylformamide / 20 h / 130 °C 2: 82 percent / H2; HCl / Pd/C / ethanol / 12 h / 20 °C 3: 87 percent / Et3N / CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Jai, Woong Seo; Srisook, Ekaruth; Hyo, Jin Son; Hwang, Onyou; Cha, Young-Nam; Dae, Yoon Chi
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 14 p. 3369 - 3373
反应条件
T=80°C; 2 h; Neat (no solvent);
参考文献
Rhodia Chimie
Patent: US6362378 B1, 2002 ;
Location in patent: Example 2 ;
参考文献
Adler; Hernestam
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 319,332
反应条件
1: 20 percent / K2CO3 / acetone / 80 °C 2: 80 percent / PPTS / tetrahydrofuran; CH2Cl2 / 20 °C View Scheme
参考文献
Brotin, Thierry; Devic, Thomas; Lesage, Anne; Emsley, Lyndon; Collet, Andre
Chemistry - A European Journal, 2001 , vol. 7, # 7 p. 1561 - 1573
反应条件
Melanocarpus albomyces laccase in 1,4-dioxane T=20°C; pH=4.5; 2 h; Enzymatic reaction; TemperaturepH-value;
参考文献
Lahtinen, Maarit; Heinonen, Petri; Oivanen, Mikko; Karhunen, Pirkko; Kruus, Kristiina; Sipilae, Jussi
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 33 p. 5454 - 5464
反应条件
Melanocarpus albomyces laccase in 1,4-dioxane T=20°C; pH=4.5; 2 h; Enzymatic reaction; TemperaturepH-value;
参考文献
Lahtinen, Maarit; Heinonen, Petri; Oivanen, Mikko; Karhunen, Pirkko; Kruus, Kristiina; Sipilae, Jussi
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 33 p. 5454 - 5464
反应条件
Melanocarpus albomyces laccase; oxygen in 1,4-dioxane 24 h; sodium succinate buffer;
参考文献
Maarit, Lahtinen; Kristiina, Kruus; Petri, Heinonen; Jussi, Sipilae
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 18 p. 8357 - 8365
