4'-羟基-3'-甲氧基苯乙酮合成路线 （共 147 条）
反应条件
water; HUSY (Si/Al=15) T=250°C; P=5250.53 Torr; 2 h; Inert atmosphere; Product distribution / selectivity;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: US2012/302796 A1, 2012 ;
Location in patent: Page/Page column 6; 7 ;
反应条件
1: 81 percent 2: 91 percent / H2 / palladium on charcoal / ethanol 3: 66 percent / M-sulphuric acid / Heating View Scheme
参考文献
Herbert, Richard B.; Jackson, Frederick B.; Nicolson, Ian T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 825 - 831
反应条件
1: 91 percent / H2 / palladium on charcoal / ethanol 2: 66 percent / M-sulphuric acid / Heating View Scheme
参考文献
Herbert, Richard B.; Jackson, Frederick B.; Nicolson, Ian T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 825 - 831
反应条件
lyophilised cells of Escherichia coli overexpressing the solvent-tolerant alcohol dehydrogenase from Rhodococcus ruber DSM44541 in aq. buffer T=30°C; pH=7.5; 24 h; Resolution of racemateEnzymatic reaction;
参考文献
Paul, Caroline E.; Lavandera, Ivan; Gotor-Fernandez, Vicente; Kroutil, Wolfgang; Gotor, Vicente
ChemCatChem, 2013 , vol. 5, # 12 p. 3875 - 3881
反应条件
sulfuric acid Heating;
参考文献
Herbert, Richard B.; Jackson, Frederick B.; Nicolson, Ian T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 825 - 831
反应条件
salcomine; oxygen in methanol T=25°C; P=7600 Torr; 72 h;
参考文献
Bassoli, Angela; Gregorio, Giuseppina Di; Rindone, Bruno; Tollari, Stefano; Chioccara, Francesco; Salmona, Mario
Gazzetta Chimica Italiana, 1988 , vol. 118, # 11 p. 763 - 768
反应条件
1: 69 percent / Br2 / CHCl3; CCl4 / 1) 5 deg C, 20 min, 2) 5 deg C -> 40 deg C, 2 h 2: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C 3: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 4: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 5: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 2: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 95 percent / K2CO3 / dimethylformamide / 2 h / 25 °C 2: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 3: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 4: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
反应条件
1: 1) K2CO3, 2) 1 M NaOH / 1) DMSO, 25 deg C, 10 min, 2) DMSO, H2O, 25 deg C, 1 h 2: 78 percent / NaBH4 / ethanol / 3 h / 5 - 25 °C 3: 30 percent Chromat. / O2, Rose Bengal / acetonitrile / 13 °C / Irradiation View Scheme
参考文献
Crestini, Claudia; D'Auria, Maurizio
Tetrahedron, 1997 , vol. 53, # 23 p. 7877 - 7888
