4'-羟基-3'-甲氧基苯乙酮合成路线 （共 147 条）
参考文献
Journal of the Chemical Society, , vol. 93, p. 1522
反应条件
sodium carbonate; dimethyl sulfate in water
反应条件
acetic acid; zinc T=70°C; 6 h; Reflux;
参考文献
Chittimalla, Santhosh Kumar; Bandi, Chennakesavulu; Putturu, Sireesha; Kuppusamy, Rajesh; Boellaard, Kevin Christopher; Tan, David Chu Aan; Lum, Demi Ming Jie
European Journal of Organic Chemistry, 2014 , vol. 2014, # 12 p. 2565 - 2575
反应条件
hydrogenchloride in ligroin; water; benzene
参考文献
A. H. Robins Company, Incorporated
Patent: US4950674 A1, 1990 ;
反应条件
isopropyl alcohol 1.5 h; Reflux;
参考文献
Zuidema, Daniel R.; Williams, Sarah L.; Wert, Katherine J.; Bosma, Karin J.; Smith, Abigail L.; Mebane, Robert C.
Synthetic Communications, 2011 , vol. 41, # 19 p. 2927 - 2931
反应条件
1.1: copper(I) bromide / ethanol 2.1: sodium / ethanol 2.2: Cooling with ice 3.1: potassium carbonate / ethanol / 2 h / 49.84 °C 4.1: sodium tetrahydroborate; sodium hydroxide / 20 °C 5.1: ; hydrogen / ethylene glycol / 199.84 °C / 37503.8 Torr / Autoclave View Scheme
参考文献
Song, Qi; Wang, Feng; Xu, Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7019 - 7021
反应条件
T=150 - 190°C; unter Druck.Hydrogenation;
参考文献
Harris; Saeman; Bergstrom
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 2063,2065
Full Text Show Details
Pepper; Hibbert
Journal of the American Chemical Society, 1948 , vol. 70, p. 67,70
反应条件
hydrogenchloride; sodium cyanoborohydride in methanol 18 h; Product distribution;
参考文献
Elliger, Carl A.
Synthetic Communications, 1985 , vol. 15, # 14 p. 1315 - 1324
反应条件
1.1: copper(I) bromide / ethanol 2.1: sodium / ethanol 2.2: Cooling with ice 3.1: potassium carbonate / ethanol / 2 h / 49.84 °C 4.1: sodium tetrahydroborate; sodium hydroxide / 20 °C 5.1: 10 palladium on activated charcoal; hydrogen / ethylene glycol / 199.84 °C / 37503.8 Torr / Autoclave View Scheme
参考文献
Song, Qi; Wang, Feng; Xu, Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7019 - 7021
反应条件
1.1: copper(I) bromide / ethanol 2.1: sodium / ethanol 2.2: Cooling with ice 3.1: potassium carbonate / ethanol / 2 h / 49.84 °C 4.1: sodium tetrahydroborate; sodium hydroxide / 20 °C 5.1: ; hydrogen / ethylene glycol / 199.84 °C / 37503.8 Torr / Autoclave View Scheme
参考文献
Song, Qi; Wang, Feng; Xu, Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7019 - 7021
