1: 96 percent / AgOTf; pyridine / 1 h / 20 °C 2: 38 percent / DBU / toluene / 96 h / 80 °C 3: 84 percent / Me3P / H2O; tetrahydrofuran / 16 h / 0 - 55 °C 4: 98 percent / TBAF; AcOH / tetrahydrofuran / 2 h / 0 °C View Scheme
参考文献
Van Den Berg, Richard J.B.H.N.; Korevaar, Cornelis G.N.; Van Der Marel, Gijsbert A.; Overkleeft, Herman S.; Van Boom, Jacques H.
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8409 - 8412
1: 96 percent / AgOTf; pyridine / 1 h / 20 °C 2: 38 percent / DBU / toluene / 96 h / 80 °C 3: 99 percent / TBAF; AcOH / tetrahydrofuran / 2 h / 0 °C View Scheme
参考文献
Van Den Berg, Richard J.B.H.N.; Korevaar, Cornelis G.N.; Van Der Marel, Gijsbert A.; Overkleeft, Herman S.; Van Boom, Jacques H.
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8409 - 8412
