phosphorus tribromide in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Kim, Sung Kuk; Gross, Dustin E.; Cho, Dong-Gyu; Lynch, Vincent M.; Sessler, Jonathan L.
Journal of Organic Chemistry, 2011 , vol. 76, # 4 p. 1005 - 1012
1: sodium hydroxide / 1,2-dichloro-ethane / 48 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C
3: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
Kim, Sung Kuk; Gross, Dustin E.; Cho, Dong-Gyu; Lynch, Vincent M.; Sessler, Jonathan L.
Journal of Organic Chemistry, 2011 , vol. 76, # 4 p. 1005 - 1012
1: sodium hydroxide / 1,2-dichloro-ethane / 48 h / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C
3: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
Kim, Sung Kuk; Gross, Dustin E.; Cho, Dong-Gyu; Lynch, Vincent M.; Sessler, Jonathan L.
Journal of Organic Chemistry, 2011 , vol. 76, # 4 p. 1005 - 1012
