反应条件
1: 1.) DMAP, 2.) AlCl3 / 1.) CHCl3, reflux, 2.5 h, 2.) 1,2-dichloroethane, room temperature, 10 min
2: LiAlH4 / diethyl ether / 0.17 h / Heating
3: 5.2 g / K5IO6, aq. H2SO4 / ethanol / 1.) 0 deg C, 2 h, 2.) 0 deg C to room temperature
4: 9.5 g / K2CO3 / acetone / 3 h / Heating
5: LiCl / H2O; dimethylsulfoxide / 2 h / 165 °C
6: LiAlH4 / diethyl ether / 2 h / Heating
7: MnO2 / benzene / 12 h / Heating
View Scheme
参考文献
Sargent, Melvyn V.; Stransky, Peter O.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 7 p. 1605 - 1610
