in ethanol prepn. by refluxing ZnO with excess of carboxylic acid in EtOH for about2 h; cooled; ppt. filtered off; washed (EtOH) repeatedly; collected; kept over silica gel in vac. desiccator; elem. anal.;
参考文献
Taylor, Richard A.; Ellis, Henry A.
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 1 p. 99 - 107
H2O2; electrogalvanized steel in water Kinetics; carboxylation in bath of water/3-methoxy-3-methyl-1-butanol (50:50 v/v) at 55 °C in presence of H2O2; detd. by XRD;
参考文献
Mesbah, Adel; Jacques, Sophie; Rocca, Emmanuel; Francois, Michel; Steinmetz, Jean
European Journal of Inorganic Chemistry, 2011 , # 8 p. 1315 - 1321
in ethanol; water stoich. amt. of aq. soln. of ZnCl2 added to alcoholic soln. of org. compd.; ppt. filtered and washed with EtOH and water, characterized by powder XRD patterns;
参考文献
Barman; Vasudevan
Journal of Physical Chemistry B, 2006 , vol. 110, # 45 p. 22407 - 22414
