反应条件
1: methylmagnesium bromide; benzyl (2R,4S,5R)-4-methyl-5-phenyl-1,2,3-oxathiazolidine-2-oxide-3-carboxilate in dichloromethane
T=-78°C;
2: With tetrafluoroboric acid in dichloromethane
T=-20°C; 0.0833333 h;
3: 2,4,6-trimethylphenylmagnesium bromide in dichloromethane
T=-20°C; Further stages. Title compound not separated from byproducts.;
参考文献
Ruano, Jose L. Garcia; Alemparte, Carlos; Aranda, M. Teresa; Zarzuelo, Maria M.
Organic Letters, 2003 , vol. 5, # 1 p. 75 - 78