(4-氯苯基)-氧代乙醛合成路线 (共 25 条)
反应条件
2: mcpba 3: 69 percent / CH2Cl2; dimethylformamide View Scheme
参考文献
Taylor, Edward C.; Pont, Joseph L.
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 379 - 382
反应条件
aluminium trichloride T=0°C;
参考文献
Arnold; Fuson
Journal of the American Chemical Society, 1936 , vol. 58, p. 1295
参考文献
Arnold; Fuson
Journal of the American Chemical Society, 1936 , vol. 58, p. 1295
反应条件
1: in tetrahydrofuran; methanol T=0°C; 0.166667 h; 2: With sodium tetrahydroborate in tetrahydrofuran; methanol 3: With hydrogenchloride; sodium hydroxide more than 3 stages;
参考文献
MITSUBISHI PHARMA CORPORATION; SANOFI-SYNTHELABO
Patent: WO2004/85408 A1, 2004 ;
Location in patent: Page 275 ;
WO 2004/085408 A1
参考文献
Young, Ryan M.; Davies-Coleman, Michael T.
Tetrahedron Letters, 2011 , vol. 52, # 31 p. 4036 - 4038
反应条件
sodium acetate in acetic acid
参考文献
Massarani; Nardi; Pozzi; Degen
Journal of medicinal chemistry, 1970 , vol. 13, # 1 p. 157 - 159
反应条件
sodium acetate in acetic acid
参考文献
Journal of medicinal chemistry, , vol. 13, # 1 p. 157 - 159
反应条件
1-amino-2-oxo-4,6-diphenylpyridine in toluene T=110°C; 6 h;
参考文献
Alajarin, M.; Fresneda, P. M.; Molina, P.
Synthesis, 1980 , # 10 p. 844 - 845
反应条件
hydrogen bromide; dimethyl sulfoxide
T=55°C; 1.5 h;
参考文献
Tanaka; Kawano; Islam; Nishioka; Hatanaka; Ueda
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 5 p. 885 - 891
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Yang, Yan; Gao, Meng; Deng, Cong; Zhang, Dong-Xue; Wu, Liu-Ming; Shu, Wen-Ming; Wu, An-Xin
Tetrahedron, 2012 , vol. 68, # 31 p. 6257 - 6262