1: With tetrafluoroboric acid; iodobenzene; 3-chloro-benzenecarboperoxoic acid in dichloromethane; water T=25°C; Hofmann rearrangement; 48 h; Inert atmosphere; 2: With hydrogenchloride in dichloromethane; water Inert atmosphere;
参考文献
Miyamoto, Kazunori; Sakai, Yuuta; Goda, Shunsuke; Ochiai, Masahito
Chemical Communications, 2012 , vol. 48, # 7 p. 982 - 984
1: With iron (III) acetylacetonate; hydrazine hydrate in methanol T=150°C; 0.0333333 h; Microwave irradiation; 2: With hydrogenchloride in water; ethyl acetate chemoselective reaction;
参考文献
Cantillo, David; Moghaddam, Mojtaba Mirhosseini; Kappe, C. Oliver
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4530 - 4542