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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
胸苷
合成路线
（共 434 条）
35002-94-9
[(2R,3S,5R)-3-羟基-5-(5-甲基-2,4-二氧代嘧啶-1-基)四氢呋喃-2-基]甲基[(2R,3S,5R)-2-(羟基甲基)-5-(5-甲基-2,4-二氧代嘧啶-1-基)四氢呋喃-3-基]甲基磷酸酯
→
反应条件
74584-62-6
+
55728-65-9
+
1969-54-6
胸苷酰(3'->5')胸苷铵盐
+
50-89-5
胸苷
反应条件
sodium hydroxide T=37°C; 24 h;
参考文献
Jankowski, Aleksander; Golankiewicz, Krzysztof
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1563 - 1568
365-07-1
胸苷酸
→
反应条件
50-89-5
胸苷
反应条件
cerium(III) chloride; HEPES buffer; oxygen in water T=50°C; Rate constant;
参考文献
Sumaoka, Jun; Kajimura, Ayako; Imai, Takamitsu; Ohno, Masayuki; Komiyama, Makoto
Nucleosides and Nucleotides, 1998 , vol. 17, # 1-3 p. 613 - 623
87367-14-4
→
反应条件
反应条件
hydroxide in water T=80°C; Hydrolysis; pH=14; Kinetics;
参考文献
Takeda, Naoya; Shibata, Masahiko; Tajima, Nobuo; Hirao, Kimihiko; Komiyama, Makoto
Journal of Organic Chemistry, 2000 , vol. 65, # 14 p. 4391 - 4396
855743-29-2
→
反应条件
50-89-5
胸苷
反应条件
in methanol UV-irradiation; Quantum yieldProduct distribution; Further Variations:irradiation wave-length;
参考文献
Woell, Dominik; Smirnova, Julia; Galetskaya, Marina; Prykota, Tamara; Buehler, Jochen; Stengele, Klaus-Peter; Pfleiderer, Wolfgang; Steiner, Ulrich E.
Chemistry - A European Journal, 2008 , vol. 14, # 21 p. 6490 - 6497
777864-69-4
→
反应条件
50-89-5
胸苷
反应条件
in methanol UV-irradiation; Quantum yieldProduct distribution; Further Variations:irradiation wave-length;
参考文献
Woell, Dominik; Smirnova, Julia; Galetskaya, Marina; Prykota, Tamara; Buehler, Jochen; Stengele, Klaus-Peter; Pfleiderer, Wolfgang; Steiner, Ulrich E.
Chemistry - A European Journal, 2008 , vol. 14, # 21 p. 6490 - 6497
777864-75-2
→
反应条件
50-89-5
胸苷
反应条件
in methanol UV-irradiation; Quantum yieldProduct distribution; Further Variations:irradiation wave-length;
参考文献
Woell, Dominik; Smirnova, Julia; Galetskaya, Marina; Prykota, Tamara; Buehler, Jochen; Stengele, Klaus-Peter; Pfleiderer, Wolfgang; Steiner, Ulrich E.
Chemistry - A European Journal, 2008 , vol. 14, # 21 p. 6490 - 6497
124130-15-0
→
反应条件
50-89-5
胸苷
反应条件
1: 92 percent / NaOH; pyridine 2: 82 percent / benzyl alcohol / 30 h / 90 °C View Scheme
参考文献
Maguire, Anita R.; Hladezuk, Isabelle; Ford, Alan
Carbohydrate Research, 2002 , vol. 337, # 4 p. 369 - 372
1397775-96-0
→
反应条件
1443257-88-2
+
1443257-87-1
+
5116-24-5
5-羟甲基脱氧尿苷
+
50-89-5
胸苷
反应条件
1: water; trifluoroacetic acid / dichloromethane / 4 h / 0 °C / |Inert atmosphere 2: tetrabutyl ammonium fluoride / tetrahydrofuran / |Inert atmosphere 3: water / 0.17 h / |UV-irradiation; |Inert atmosphere View Scheme
参考文献
Lin, Gengjie; Li, Lei
Angewandte Chemie - International Edition, 2013 , vol. 52, # 21 p. 5594 - 5598
Angew. Chem., 2013 , vol. 125, # 21 p. 5704 - 5708,5
40733-26-4
3,5-双-o-(t-丁基二甲基甲硅烷基)胸腺嘧啶脱氧核苷
→
反应条件
1443257-88-2
+
1443257-87-1
+
5116-24-5
5-羟甲基脱氧尿苷
+
50-89-5
胸苷
反应条件
1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / |Inert atmosphere; |Reflux 2: triethylamine / N,N-dimethyl-formamide / 24 h / 70 °C / |Inert atmosphere 3: water; trifluoroacetic acid / dichloromethane / 4 h / 0 °C / |Inert atmosphere 4: tetrabutyl ammonium fluoride / tetrahydrofuran / |Inert atmosphere 5: water / 0.17 h / |UV-irradiation; |Inert atmosphere View Scheme
参考文献
Lin, Gengjie; Li, Lei
Angewandte Chemie - International Edition, 2013 , vol. 52, # 21 p. 5594 - 5598
Angew. Chem., 2013 , vol. 125, # 21 p. 5704 - 5708,5
291525-17-2
→
反应条件
1443257-88-2
+
1443257-87-1
+
5116-24-5
5-羟甲基脱氧尿苷
+
50-89-5
胸苷
反应条件
1: triethylamine / N,N-dimethyl-formamide / 24 h / 70 °C / |Inert atmosphere 2: water; trifluoroacetic acid / dichloromethane / 4 h / 0 °C / |Inert atmosphere 3: tetrabutyl ammonium fluoride / tetrahydrofuran / |Inert atmosphere 4: water / 0.17 h / |UV-irradiation; |Inert atmosphere View Scheme
参考文献
Lin, Gengjie; Li, Lei
Angewandte Chemie - International Edition, 2013 , vol. 52, # 21 p. 5594 - 5598
Angew. Chem., 2013 , vol. 125, # 21 p. 5704 - 5708,5
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