1: 7.8 g / copper powder, anhydrous potassium carbonate / dimethylformamide / 10 h / Heating
2: 6 g / polyphosphoric acid / 3 h / 110 °C
3: 1.68 g / pyridine hydrochloride / 2 h / 230 °C
4: 192 mg / anhydrous potassium carbonate, anhydrous sodium iodide / dimethylformamide / 20 h / 70 °C
View Scheme
参考文献
Reisch, Johannes; Mester, Iuliu; Aly, Samir M. El-Moghazy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 219 - 223
1: 7.8 g / copper powder, anhydrous potassium carbonate / dimethylformamide / 10 h / Heating
2: 6 g / polyphosphoric acid / 3 h / 110 °C
3: 1.68 g / pyridine hydrochloride / 2 h / 230 °C
View Scheme
参考文献
Reisch, Johannes; Mester, Iuliu; Aly, Samir M. El-Moghazy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 219 - 223
1: 3,5-dimethoxy-phenol With potassium carbonate in acetone
T=60°C; 0.666667 h; Inert atmosphere;
2: α-bromo-4-methylacetophenone in acetone
T=60°C; 12 h; Inert atmosphere;
参考文献
Correa, Christian; Cruz, Maria Del Carmen; Jimnez, Fabiola; Zepeda, L. Gerardo; Tamariz, Joaqun
Australian Journal of Chemistry, 2008 , vol. 61, # 12 p. 991 - 999