反应条件
1: piperazine-1-carboxylic acid tert-butyl ester With sodium hydride in DMF (N,N-dimethyl-formamide)
T=0 - 20°C; 1 h;
2: [3-(bromomethyl)-phenoxy]dimethyl(1,1-dimethylethyl)silane in DMF (N,N-dimethyl-formamide)
T=20°C; 24 h;
3: With water in DMF (N,N-dimethyl-formamide)
0.5 h;