in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) byproducts: C6H5CH2CH2CH2SCH3; to soln. of Pd(CH2CH2CH2C6H5)2(dppe) in THF/THF-d8 (4:1) added CH3SSCH3 at 15°C under Ar, mixture transferred to NMR tube for 6 days; not isolated, identified by NMR;

in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) byproducts: CH3CH2CH2C6H5; to soln. of Pd(CH2CH2CH2C6H5)2(dppe) in THF/THF-d8 (4:1) added (CH3)2CHSH under Ar, mixture transferred to NMR tube, 6 days at -30°C, 1 day at -15°C, 8 days at 0°C; not isolated, identified by NMR;

in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) byproducts: CH3CH2CH2C6H5; to soln. of Pd(CH2CH2CH2C6H5)2(dppe) in THF/THF-d8 (4:1) added (CH3)3CSHunder Ar, mixture transferred to NMR tube, 6 days at -30°C, 1 da y at -15°C, 8 days at 0°C; not isolated, identified by NMR;

in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) byproducts: CH3SeCH2CH2CH2C6H5; to soln. of Pd(CH2CH2CH2C6H5)2(dppe) in THF/THF-d8 (4:1) added (CH3Se)2 at -30°C under Ar, mixture transferred to NMR tube for 2 days; not isolated, identified by NMR;