二甲基5-硫代-1,3-吡咯烷二羧酸酯合成路线 (共 2 条)
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 12 h;
参考文献
Stanetty, Peter; Turner, Martin; Mihovilovic, Marko D.
Molecules, 2005 , vol. 10, # 2 p. 367 - 375
反应条件
1: 99 percent / Lawesson's reagent / tetrahydrofuran / 2 h / 20 °C
2: 30 percent / triethylamine; DMAP / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Stanetty, Peter; Turner, Martin; Mihovilovic, Marko D.
Molecules, 2005 , vol. 10, # 2 p. 367 - 375