4-苯基-1(2H)-酞嗪酮合成路线 (共 19 条)
反应条件
sodium acetate; monohydrazine sulfate in water
参考文献
Yamada; Nobuhara; Yamaguchi; Ohki
Journal of Medicinal Chemistry, 1982 , vol. 25, # 8 p. 975 - 982
参考文献
Johnson, Robert E.; Hane, Jeffrey T.; Schlegel, Donald C.; Perni, Robert B.; Herrmann, John L.; et al.
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5218 - 5221
反应条件
hydrazine hydrate in N,N-dimethyl-formamide 20 h; Heating;
参考文献
Wharton, Clifford J.; Wrigglesworth, Roger
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 809 - 814
反应条件
hydrogenchloride in ethanol 36 h; Heating;
参考文献
Richter; Kasbohm; Besch; Hagen
Pharmazie, 1992 , vol. 47, # 10 p. 758 - 764
反应条件
1: 73 percent / ethanol / 2 h / Heating 2: 57 percent / diethyl ether; benzene / 6 h / Heating View Scheme
参考文献
Ismail, Mohamed Fekry; Kandile, Nadia Gharib
Acta Chimica Hungarica, 1991 , vol. 128, # 2 p. 251 - 253
反应条件
aluminium trichloride Ambient temperature;
参考文献
Derbala, H. A. Y.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 8 p. 779 - 781
反应条件
in diethyl ether; benzene 6 h; Heating;
参考文献
Derbala, H. A. Y.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 8 p. 779 - 781
反应条件
1: 54 percent / tetrahydrofuran; cyclohexane; diethyl ether / -40 deg C, 40 min, room temp., 17 h 2: 49 percent / hydrazine hydrate / dimethylformamide / 20 h / Heating View Scheme
参考文献
Wharton, Clifford J.; Wrigglesworth, Roger
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 809 - 814
反应条件
1: 54 percent / tetrahydrofuran; cyclohexane; diethyl ether / -40 deg C, 40 min, room temp., 17 h 2: 49 percent / hydrazine hydrate / dimethylformamide / 20 h / Heating View Scheme
参考文献
Wharton, Clifford J.; Wrigglesworth, Roger
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 809 - 814
反应条件
AlCl3, aluminium chloride in dichloromethane 4 h; Reflux;
参考文献
Derbala, Hamed A.
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 3 p. 700 - 704