双(9,9-二甲基-9H-芴-2-基)胺合成路线 （共 3 条）
反应条件
trifluoroacetic acid in tetrahydrofuran
T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Samsung SDI Co., Ltd.
Patent: EP2371813 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate in toluene
T=85°C; 3 h;
参考文献
Samsung Display Co., Ltd.; Kim, Young-Kook; Hwang, Seok-Hwan; Jung, Hye-Jin; Lim, Jin-O; Han, Sang-Hyun; Cho, Se-Jin; Lee, Jong-Hyuk
Patent: EP2581365 A1, 2013 ;
Location in patent: Paragraph 0129 ;
反应条件
1: copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine / tetrahydrofuran / 36 h / 80 °C / Inert atmosphere
2: trifluoroacetic acid / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Cho, Nara; Choi, Hyunbong; Kim, Duckhyun; Song, Kihyung; Kang, Moon-sung; Kang, Sang Ook; Ko, Jaejung
Tetrahedron, 2009 , vol. 65, # 31 p. 6236 - 6243
