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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
白藜芦醇
合成路线
（共 177 条）
824-94-2
4-甲氧基氯苄
→
反应条件
501-36-0
白藜芦醇
反应条件
1: Reflux 2: sodium methylate / N,N-dimethyl-formamide / 10 h / 20 °C 3: pyridine hydrochloride / 4 h / 190 - 195 °C View Scheme
参考文献
Cai, Wenqing; Zhang, Liangwei; Song, Yanlin; Zhang, Baoxin; Cui, Xuemei; Hu, Guanming; Fang, Jianguo
Free Radical Research, 2011 , vol. 45, # 11-12 p. 1379 - 1387
76280-61-0
→
反应条件
501-36-0
白藜芦醇
反应条件
1: Methyltriphenylphosphonium bromide; sodium hydride / tetrahydrofuran; mineral oil / 65 °C / |Inert atmosphere 2: sodium acetate; palladium diacetate / methanol / 12 h / 20 °C / |Inert atmosphere 3: hydrogenchloride / water; methanol / 3 h / 20 - 65 °C / |Inert atmosphere View Scheme
参考文献
Schmidt, Bernd; Elizarov, Nelli; Berger, Rene; Hoelter, Frank
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 22 p. 3674 - 3691
76280-59-6
→
反应条件
501-36-0
白藜芦醇
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 6 h / 20 °C / |Inert atmosphere 2: Dess-Martin periodane / dichloromethane / 0 °C / |Inert atmosphere 3: Methyltriphenylphosphonium bromide; sodium hydride / tetrahydrofuran; mineral oil / 65 °C / |Inert atmosphere 4: sodium acetate; palladium diacetate / methanol / 12 h / 20 °C / |Inert atmosphere 5: hydrogenchloride / water; methanol / 3 h / 20 - 65 °C / |Inert atmosphere View Scheme
参考文献
Schmidt, Bernd; Elizarov, Nelli; Berger, Rene; Hoelter, Frank
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 22 p. 3674 - 3691
76280-60-9
→
反应条件
501-36-0
白藜芦醇
反应条件
1: Dess-Martin periodane / dichloromethane / 0 °C / |Inert atmosphere 2: Methyltriphenylphosphonium bromide; sodium hydride / tetrahydrofuran; mineral oil / 65 °C / |Inert atmosphere 3: sodium acetate; palladium diacetate / methanol / 12 h / 20 °C / |Inert atmosphere 4: hydrogenchloride / water; methanol / 3 h / 20 - 65 °C / |Inert atmosphere View Scheme
参考文献
Schmidt, Bernd; Elizarov, Nelli; Berger, Rene; Hoelter, Frank
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 22 p. 3674 - 3691
1438867-27-6
→
反应条件
501-36-0
白藜芦醇
反应条件
1: sodium acetate; palladium diacetate / methanol / 12 h / 20 °C / |Inert atmosphere 2: hydrogenchloride / water; methanol / 3 h / 20 - 65 °C / |Inert atmosphere View Scheme
参考文献
Schmidt, Bernd; Elizarov, Nelli; Berger, Rene; Hoelter, Frank
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 22 p. 3674 - 3691
869011-52-9
→
反应条件
501-36-0
白藜芦醇
反应条件
1.1: NaH / tetrahydrofuran / 2 h / -55 - 0 °C 1.2: 50.8 percent / tetrahydrofuran / 24 h / -55 - 0 °C 2.1: 79 percent / hydrochloric acid / ethanol / 26 h / 20 °C View Scheme
参考文献
Takaya, Yoshiaki; Terashima, Kenji; Ito, Junko; He, Yue-Hua; Tateoka, Maki; Yamaguchi, Naho; Niwa, Masatake
Tetrahedron, 2005 , vol. 61, # 43 p. 10285 - 10290
123-08-0
对羟基苯甲醛
→
反应条件
501-36-0
白藜芦醇
反应条件
1.1: 58.1 percent / imidazole / dimethylformamide / 21 h / 20 °C 2.1: NaH / tetrahydrofuran / 2 h / -55 - 0 °C 2.2: 50.8 percent / tetrahydrofuran / 24 h / -55 - 0 °C 3.1: 79 percent / hydrochloric acid / ethanol / 26 h / 20 °C View Scheme
参考文献
Csuk, Rene; Albert, Sabrina; Kluge, Ralph; Stroehl, Dieter
Archiv der Pharmazie, 2013 , vol. 346, # 7 p. 499 - 503
103929-85-7
1-(氯甲基)-3,5-二[[(叔丁基)二甲基硅烷基]氧基]苯
→
反应条件
501-36-0
白藜芦醇
反应条件
1.1: 86.1 percent / NaI / 6 h / 135 °C 2.1: NaH / tetrahydrofuran / 2 h / -55 - 0 °C 2.2: 50.8 percent / tetrahydrofuran / 24 h / -55 - 0 °C 3.1: 79 percent / hydrochloric acid / ethanol / 26 h / 20 °C View Scheme
参考文献
Takaya, Yoshiaki; Terashima, Kenji; Ito, Junko; He, Yue-Hua; Tateoka, Maki; Yamaguchi, Naho; Niwa, Masatake
Tetrahedron, 2005 , vol. 61, # 43 p. 10285 - 10290
71135-82-5
→
反应条件
501-36-0
白藜芦醇
反应条件
1.1: LDA / tetrahydrofuran / 0 - 20 °C 1.2: I2 / heptane / 12 h / Heating 2.1: HCl / methanol / 36 h / 20 °C View Scheme
参考文献
Lee, Hyun Jung; Seo, Jai Woong; Lee, Bong Ho; Chung, Kyoo-Hyun; Chi, Dae Yoon
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 2 p. 463 - 466
158139-69-6
→
反应条件
501-36-0
白藜芦醇
反应条件
1.1: tetrahydrofuran / Heating 2.1: LDA / tetrahydrofuran / 0 - 20 °C 2.2: I2 / heptane / 12 h / Heating 3.1: HCl / methanol / 36 h / 20 °C View Scheme
参考文献
Lee, Hyun Jung; Seo, Jai Woong; Lee, Bong Ho; Chung, Kyoo-Hyun; Chi, Dae Yoon
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 2 p. 463 - 466
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