3,7-二甲基-6-辛烯酸合成路线 （共 32 条）
反应条件
an der Luft; dextrorotatory 2,6-dimethyl-octen-(2)-oic acid (8);
参考文献
Verley
Bulletin de la Societe Chimique de France, 1925 , vol. <4>37, p. 539
反应条件
ethanol und Erwaermen des Reaktionsprodukts mit wss.Natronlauge und Erhitzen der nach dem Ansaeuern erhaltenen Dicarbonsaeure bis auf 155grad;
参考文献
Ofner et al.
Helvetica Chimica Acta, 1959 , vol. 42, p. 2577,2582
反应条件
sodium ethanolate T=110°C;
参考文献
Bouveault; Blanc
Patent: DE164294 ;
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Bouveault; Gourmand
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1904 , vol. 138, p. 1701
Chem. Zentralbl., 1905 , vol. 76, # II p. 1701
参考文献
Charlton, James Leslie.; Lai, Hoi Kiong.; Lypka, Gerald Nicholas
Canadian Journal of Chemistry, 1980 , vol. 58, p. 458 - 462
反应条件
2: 85 percent 3: 1. sodium methaperiodate 2. reflux, toluene, 20 h, CaCO3 View Scheme
参考文献
Fujisawa, Tamotsu; Sato, Toshio; Kawara, Tatsuo; Noda, Atsunari; Obinata,Toshiyuki
Tetrahedron Letters, 1980 , vol. 21, p. 2553 - 2554
反应条件
inactive 2,6-dimethyl-octen-(2)-oic acid (8);
参考文献
Wallach
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 130
反应条件
1: SOCl2 / pyridine 2: 1. BF3*OEt2, CH2Cl2, room temperature, 2 day 2. K2CO3, methanol, room temperature, 3 h View Scheme
参考文献
Barczak, Nicholas T.; Jarvo, Elizabeth R.
Chemistry - A European Journal, 2011 , vol. 17, # 46 p. 12912 - 12916
反应条件
2: 85 percent 3: 1. sodium methaperiodate 2. reflux, toluene, 20 h, CaCO3 4: LiAlH4 View Scheme
参考文献
Fujisawa, Tamotsu; Sato, Toshio; Kawara, Tatsuo; Noda, Atsunari; Obinata,Toshiyuki
Tetrahedron Letters, 1980 , vol. 21, p. 2553 - 2554
反应条件
2: 85 percent 3: 1. sodium methaperiodate 2. reflux, toluene, 20 h, CaCO3 4: LiAlH4 View Scheme
参考文献
Fujisawa, Tamotsu; Sato, Toshio; Kawara, Tatsuo; Noda, Atsunari; Obinata,Toshiyuki
Tetrahedron Letters, 1980 , vol. 21, p. 2553 - 2554
反应条件
inactive 2,6-dimethyl-octen-(2)-oic acid (8);
参考文献
Wallach
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 130
