3,7,11-三甲基-1,3,6,10-十二碳-四烯合成路线 （共 28 条）
反应条件
pyridine in dimethyl sulfoxide T=160°C; 0.0833333 h;
参考文献
Vander Meer; Williams; Lofgren
Tetrahedron Letters, 1981 , vol. 22, # 18 p. 1651 - 1654
反应条件
Dowex 50W-X4 cation exchange resin in hexane 4 h; Heating;
参考文献
Brieger,G. et al.
Journal of Organic Chemistry, 1969 , vol. 34, p. 3789 - 3791
反应条件
in xylene 0.0833333 h; Heating;
参考文献
Fielder; Rowan
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 11 p. 1075 - 1085
反应条件
1: KOH 2: RhCl2 / ethanol View Scheme
参考文献
Brieger,G. et al.
Journal of Organic Chemistry, 1969 , vol. 34, p. 3789 - 3791
反应条件
1: 72 percent / BuLi / hexane; diethyl ether / 1.) 20 deg C, 15 min, 2.) -78 deg C, 30 min; r.t., 30 min 2: LDA / diethyl ether / 1.) 0 deg C, 30 min, 2.) -78 deg C, 30 min; 25 deg C, 30 min 3: NaH / dimethylformamide View Scheme
参考文献
Spicer, Julie A.; Brimble, Margaret A.; Rowan, Daryl D.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1929 - 1940
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Faraldos, Juan A.; Gonzalez, Veronica; Senske, Michael; Allemann, Rudolf K.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6920 - 6923
反应条件
1: LDA / diethyl ether / 1.) 0 deg C, 30 min, 2.) -78 deg C, 30 min; 25 deg C, 30 min 2: NaH / dimethylformamide View Scheme
参考文献
Ramaiah; Pegram; Millar
Journal of Organic Chemistry, 1995 , vol. 60, # 19 p. 6211 - 6213
反应条件
rhodium(II) chloride in ethanol
参考文献
Brieger,G. et al.
Journal of Organic Chemistry, 1969 , vol. 34, p. 3789 - 3791
反应条件
rhodium(II) chloride in ethanol
参考文献
Brieger,G. et al.
Journal of Organic Chemistry, 1969 , vol. 34, p. 3789 - 3791
反应条件
tetrakis(triphenylphosphine) palladium(0); zirconocene dichloride 1.) 1,2-dichloroethane, xylene, room temperature, 12 h, 2.) THF, room temperature, 3 h; Yield given. Multistep reaction;
参考文献
Matsushita,H.; Negishi,E.I.
Journal of the American Chemical Society, 1981 , vol. 103, p. 2882
