3,7,11-三甲基-1,3,6,10-十二碳-四烯合成路线 （共 28 条）
反应条件
pyridine; trichlorophosphate 1) ice bath, 1 h; 2) rt, 12 h; Title compound not separated from byproducts;
参考文献
Svatos; Attygalle
Analytical chemistry, 1997 , vol. 69, # 10 p. 1827 - 1836
反应条件
dimethyl sulfoxide Heating;
参考文献
Courtney,J.L.; McDonald,S.
Australian Journal of Chemistry, 1969 , vol. 22, p. 2411 - 2416
参考文献
Larkin,J.P. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2524 - 2528
反应条件
n-butyllithium 1.) THF, pentane, RT, 2.) THF, pentane, -78 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Fielder; Rowan
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 11 p. 1075 - 1085
反应条件
hydrogen; palladium T=140°C;
参考文献
Attygalle, Athula B.; Morgan, E. David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 949 - 952
反应条件
1: 31 percent / mCPBA / CH2Cl2 / Ambient temperature 2: 42 percent / periodic acid / tetrahydrofuran / 0.03 h / Ambient temperature View Scheme
参考文献
Fielder; Rowan
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 11 p. 1075 - 1085
反应条件
3,5-dimethyl-1H-pyrazole; chromium(VI) oxide in dichloromethane 2 h;
参考文献
Spicer, Julie A.; Brimble, Margaret A.; Rowan, Daryl D.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1929 - 1940
反应条件
ozone
T=200°C; 0.0833333 h; Product distribution;
参考文献
Attygalle, Athula B.; Morgan, E. David
Analytical Chemistry, 1983 , vol. 55, # 8 p. 1379 - 1384
