反应条件
1: 3,7,11-trimethyl-1,3,6,10-tetraene-dodecyl diethyl phosphonate With potassium tert-butylate in tetrahydrofuran; dimethyl sulfoxide T=5°C; 2 h; Inert atmosphere; 2: 2,7-dimethylocta-2,4,6-triene-1,8-dial in tetrahydrofuran; dimethyl sulfoxide T=5 - 25°C; 1.58 h; 3: in chloroform 2 h; RefluxInert atmosphere;
参考文献
University of Shaoxing; Zhejiang Medicine Co., Ltd., Xinchang Pharmaceutic al Factory; Lao, Xuejun; Shen, Runpu; Ye, Weidong; Song, Xiaohua; Liu, Luo; Wu, Chunlei; Sun, Xiongsheng; Hu, Siping
Patent: US2013/46114 A1, 2013 ;
Location in patent: Paragraph 0052-0055 ;