2-乙基-1H-异吲哚-1,3(2H)-二酮合成路线 （共 56 条）
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,3-bis-(diphenylphosphino)propane; hydrogen in water; toluene T=120°C; P=7500.75 Torr; 20 h; regioselective reaction;
参考文献
Uhlemann, Marcus; Doerfelt, Stephan; Boerner, Armin
Tetrahedron Letters, 2013 , vol. 54, # 18 p. 2209 - 2211
反应条件
Decaborane; palladium on activated charcoal in methanol T=25°C; Reduction; 2.5 h;
参考文献
Lee, Seung Hwan; Park, Yong June; Yoon, Cheol Min
Tetrahedron Letters, 2000 , vol. 41, # 6 p. 887 - 889
反应条件
hydrogenchloride T=20°C; Cyclization; solid-gas reaction; P=750.06 Torr;
参考文献
Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen
Tetrahedron, 2000 , vol. 56, # 36 p. 6899 - 6911
反应条件
potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate in 1,1-dimethylpropan-1-ol T=100°C; P=760.051 Torr; 24 h;
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
in N,N-dimethyl-formamide T=25°C; 6 h;
参考文献
Katritzky, Alan R.; Liso, Gaietano; Lunt, Edward; Patel, Ranjan C.; Thind, Sukhpal S.; Zia, Abid
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 849 - 851
反应条件
potassium hydroxide; 1-butylpyridinium tetrafluoroborate T=40°C; 5 h;
参考文献
Le, Zhang-Gao; Chen, Zhen-Chu; Hu, Yi; Zheng, Qin-Guo
Synthesis, 2004 , # 2 p. 208 - 212
反应条件
potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate in 1,1-dimethylpropan-1-ol T=100°C; P=760.051 Torr; 24 h;
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in tetrahydrofuran 0.00833333 h;
参考文献
Pasquini, M. A.; Goaller, R. Le; Pierre, J.L.
Tetrahedron, 1980 , vol. 36, # 82 p. 1223 - 1226
反应条件
potassium carbonate in water; acetone T=15°C; Irradiation;
参考文献
Griesbeck, Axel G.; Henz, Andreas; Kramer, Wolfgang; Lex, Johann; Nerowski, Frank; Oelgemoeller, Michael; Peters, Karl; Peters, Eva-Maria
Helvetica Chimica Acta, 1997 , vol. 80, # 3 p. 912 - 933
反应条件
Rh(acac)(CO)2; 3,3',5,5'-tetra(2,4-difluorophenyl)-2,2',6,6'-tetra((di-1-pyrrolylphosphino)oxy)-1,1'-biphenyl; hydrogen in toluene T=120°C; P=3800.26 Torr; 2 h; Autoclave; regioselective reaction;
参考文献
Cai, Chaoxian; Yu, Shichao; Cao, Bonan; Zhang, Xumu
Chemistry - A European Journal, 2012 , vol. 18, # 32 p. 9992 - 9998
