2-乙基-1H-异吲哚-1,3(2H)-二酮合成路线 (共 56 条)
反应条件
potassium carbonate in acetone Irradiation;
参考文献
Griesbeck, Axel G.
Chimia, 1998 , vol. 52, # 6 p. 272 - 283
反应条件
in acetone 3 h; Irradiation;
参考文献
Sato, Yasuhiko; Nakai, Hideo; Mizoguchi, Tomishige; Kawanishi, Masazumi; Hatanaka, Yasumaru; Kanaoka, Yuichi
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1263 - 1270
反应条件
1: 0.75 h / 150 °C 2: 45 percent / K2CO3 / H2O; acetone / 15 °C / Irradiation View Scheme
参考文献
Wanag; Veinbergs
Chemische Berichte, 1942 , vol. 75, p. 1558,1567
参考文献
Sakellarios
Helvetica Chimica Acta, 1946 , vol. 29, p. 1675,1677, 1681
反应条件
1: bromine / dichloromethane / 0.67 h / 0 - 20 °C 2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 20 °C View Scheme
参考文献
Tan, Ayse; Koc, Birgul; Sahin, Ertan; Kishali, Nurhan H.; Kara, Yunus
Synthesis, 2011 , # 7 p. 1079 - 1084
反应条件
1: triethylamine / toluene / 36 h / Reflux 2: bromine / dichloromethane / 0.67 h / 0 - 20 °C 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 20 °C View Scheme
参考文献
Tan, Ayse; Koc, Birgul; Sahin, Ertan; Kishali, Nurhan H.; Kara, Yunus
Synthesis, 2011 , # 7 p. 1079 - 1084
反应条件
1: thionyl chloride / 2 h / Reflux 2: potassium carbonate / tetrahydrofuran / Cooling with ice 3: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
1: potassium carbonate / tetrahydrofuran / Cooling with ice 2: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
1: potassium carbonate / tetrahydrofuran / Cooling with ice 2: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076
反应条件
1: potassium carbonate / tetrahydrofuran / Cooling with ice 2: potassium dihydrogenphosphate; Cp*Rh(MeCN)3[ClO4]2; silver carbonate / 1,1-dimethylpropan-1-ol / 24 h / 100 °C / 760.05 Torr View Scheme
参考文献
Du, Ya; Hyster, Todd K.; Rovis, Tomislav
Chemical Communications, 2011 , vol. 47, # 44 p. 12074 - 12076