2-乙基-1H-异吲哚-1,3(2H)-二酮合成路线 (共 56 条)
反应条件
1: ethanolic sodium ethylate 2: water; hydrochloric acid View Scheme
参考文献
Koermendy
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 17, p. 255,261
反应条件
water zuletzt unter Erhitzen;
参考文献
Wanag; Silaraja
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 68,73; engl. Ausg. S. 69, 73
参考文献
Graebe; Pictet
Chemische Berichte, 1884 , vol. 17, p. 1174
Justus Liebigs Annalen der Chemie, 1888 , vol. 247, p. 303
反应条件
in methanol; acetonitrile T=30°C; ΔH(excit.), ΔS(excit.); var. temp. and solvent composition; KineticsThermodynamic data;
参考文献
Kondo, Yasuhiko; Kondo, Kunio; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 6 p. 1141 - 1145
反应条件
in acetonitrile T=25°C; reaction enthalpy; Thermodynamic data;
参考文献
Kondo, Yasuhiko; Tsukamoto, Tamio; Kimura, Naoko
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 9 p. 1765 - 1769
参考文献
Blacher
Chemische Berichte, 1895 , vol. 28, p. 2358
参考文献
Gabriel
Chemische Berichte, 1891 , vol. 24, p. 1117
反应条件
1: 100 percent / 20 °C / 600.05 - 750.06 Torr 2: 18 h / 20 °C / 0.8 Torr View Scheme
参考文献
Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen
Tetrahedron, 2000 , vol. 56, # 36 p. 6899 - 6911
反应条件
1: 100 percent / 20 °C / 600.05 - 750.06 Torr 2: 18 h / 20 °C / 0.8 Torr 3: 100 percent / HCl / 20 °C / 750.06 Torr View Scheme
参考文献
Tetrahedron, , vol. 56, # 36 p. 6899 - 6911
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=25°C; Inert atmosphere;
参考文献
Das, Shoubhik; Addis, Daniele; Knoepke, Leif R.; Bentrup, Ursula; Junge, Kathrin; Brueckner, Angelika; Beller, Matthias
Angewandte Chemie - International Edition, 2011 , vol. 50, # 39 p. 9180 - 9184