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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5023-60-9
合成路线
（共 55 条）
5023-60-9
→
反应条件
350-50-5
氟甲苯
反应条件
1: CH2Cl2 / Ambient temperature 2: CsF / CH2Cl2 / 37 h / Heating View Scheme
参考文献
Ichikawa, Junji; Sugimoto, Ken-ichi; Sonoda, Takaaki; Kobayashi, Hiroshi
Chemistry Letters, 1987 , p. 1985 - 1988
5023-60-9
→
反应条件
131-58-8
2-甲基二苯甲酮
反应条件
1: palladium diacetate; silver carbonate / N,N-dimethyl acetamide / 120 °C 2: NH2NH2•xH2O / methanol / 20 °C View Scheme
参考文献
Xu, Bo; Liu, Wei; Kuang, Chunxiang
European Journal of Organic Chemistry, 2014 , vol. 2014, # 12 p. 2576 - 2583
106-38-7
对溴甲苯
+
100-39-0
溴化苄
→
反应条件
5023-60-9
反应条件
palladium diacetate; potassium carbonate; thiourea; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=20°C; 4 h; Inert atmosphere;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 839 - 845
103-19-5
对甲苯二硫醚
+
100-44-7
苄基氯
→
反应条件
5023-60-9
反应条件
RhCl(PPh3)3; hydrogen; triethylamine in tetrahydrofuran T=50°C; P=760 Torr; 24 h;
参考文献
Ajiki, Kaori; Hirano, Masao; Tanaka, Ken
Organic Letters, 2005 , vol. 7, # 19 p. 4193 - 4195
624-31-7
4-碘甲苯
+
100-39-0
溴化苄
→
反应条件
5023-60-9
反应条件
1: 1-(iodo)-4-methylbenzene With copper(l) iodide; potassium carbonate; sulfur in N,N-dimethyl-formamide T=90°C; Inert atmosphere; 2: With sodium tetrahydroborate in N,N-dimethyl-formamide T=40°C; Inert atmosphereCooling with ice; 3: benzyl bromide in N,N-dimethyl-formamide T=20°C; 5 h; Inert atmosphere;
参考文献
Jiang, Yongwen; Qin, Yuxia; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua; Ma, Dawei
Organic Letters, 2009 , vol. 11, # 22 p. 5250 - 5253
624-31-7
4-碘甲苯
+
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
tetra(n-butyl)ammonium hydroxide in water T=50°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Zhou, Xin-Feng; Feng, Yi-Si
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2562 - 2568
10381-70-1
→
反应条件
5023-60-9
反应条件
2,4-diphenyl-1,3-diselenadiphosphetane-2,4-diselenide in toluene 20 h; Heating;
参考文献
Hua, Guoxiong; Woollins, J. Derek
Tetrahedron Letters, 2007 , vol. 48, # 21 p. 3677 - 3679
100-39-0
溴化苄
+
106-45-6
4-甲苯硫酚
→
反应条件
5023-60-9
反应条件
N-benzyl-trimethylammonium hydroxide T=20°C; Neat (no solvent);
参考文献
Meshram; Reddy, B. Chennakesava; Goud, P. Ramesh
Synthetic Communications, 2009 , vol. 39, # 13 p. 2297 - 2303
624-31-7
4-碘甲苯
+
39077-95-7
→
反应条件
5023-60-9
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 19 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
106-38-7
对溴甲苯
+
100-53-8
苄硫醇
→
反应条件
5023-60-9
反应条件
1: phenylmethanethiol With sodium t-butanolate in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran 0.166667 h; Inert atmosphere; 3: para-bromotoluene With [P(t-Bu)3Pd(μ-Br)]2; lithium iodide in tetrahydrofuran T=90°C; 2 h; Inert atmosphere;
参考文献
Bastug, Gulluzar; Nolan, Steven P.
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9303 - 9308
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