palladium dihydroxide; ammonium formate in ethanol T=70°C; 2 h;

暂无反应条件数据

1: 96 percent / triethylamine / methanol / 2 h / 50 °C 2: 85 percent / BH3*THF / tetrahydrofuran / 2 h / 50 °C 3: 87 percent / DMSO; oxalyl chloride; triethylamine / CH2Cl2 / -60 - 20 °C 4: tetrahydrofuran / 2 h / -78 °C 5: 0.147 g / NaH / tetrahydrofuran; various solvent(s) / 1 h / Heating 6: 88 percent / Pd(OH)2/C; ammonium formate / ethanol / 2 h / 70 °C View Scheme

1: tetrahydrofuran / 2 h / -78 °C 2: 0.147 g / NaH / tetrahydrofuran; various solvent(s) / 1 h / Heating 3: 88 percent / Pd(OH)2/C; ammonium formate / ethanol / 2 h / 70 °C View Scheme

1: 87 percent / DMSO; oxalyl chloride; triethylamine / CH2Cl2 / -60 - 20 °C 2: tetrahydrofuran / 2 h / -78 °C 3: 0.147 g / NaH / tetrahydrofuran; various solvent(s) / 1 h / Heating 4: 88 percent / Pd(OH)2/C; ammonium formate / ethanol / 2 h / 70 °C View Scheme

1: 85 percent / BH3*THF / tetrahydrofuran / 2 h / 50 °C 2: 87 percent / DMSO; oxalyl chloride; triethylamine / CH2Cl2 / -60 - 20 °C 3: tetrahydrofuran / 2 h / -78 °C 4: 0.147 g / NaH / tetrahydrofuran; various solvent(s) / 1 h / Heating 5: 88 percent / Pd(OH)2/C; ammonium formate / ethanol / 2 h / 70 °C View Scheme