似梨木双黄酮-7-O-B-D-吡喃葡萄糖苷合成路线 （共 4 条）
反应条件
boron tribromide in dichloromethane
T=20°C; 72 h; Inert atmosphere;
参考文献
Ndoile, Monica M.; Van Heerden, Fanie R.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1346 - 1351
反应条件
1: potassium hydroxide / ethanol / |Cooling with ice
2: iodine / pyridine / 24 h / 80 °C
3: boron tribromide / dichloromethane / 72 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Ndoile, Monica M.; Van Heerden, Fanie R.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1346 - 1351
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / |Inert atmosphere
2: potassium hydroxide / ethanol / |Cooling with ice
3: iodine / pyridine / 24 h / 80 °C
4: boron tribromide / dichloromethane / 72 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Ndoile, Monica M.; Van Heerden, Fanie R.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1346 - 1351
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / |Inert atmosphere
2: potassium hydroxide / ethanol / |Cooling with ice
3: iodine / pyridine / 24 h / 80 °C
4: boron tribromide / dichloromethane / 72 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Ndoile, Monica M.; Van Heerden, Fanie R.
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1346 - 1351
