2-(4-甲基哌嗪)-3-氨基吡啶合成路线 （共 6 条）
反应条件
ammonium formate; palladium 10 on activated carbon in methanol T=20°C; 1 h;
参考文献
PFIZER PRODUCTS INC.
Patent: WO2006/48727 A1, 2006 ;
Location in patent: Page/Page column 72-73 ;
WO 2006/048727 A1
反应条件
hydrazine hydrate; calcium carbonate; palladium on activated charcoal in ethanol 2 h; Heating;
参考文献
Dunn
Organic Preparations and Procedures International, 1998 , vol. 30, # 6 p. 709 - 713
反应条件
1: 71 percent / 1 h / Heating 2: 70 percent / CaCO3, hydrazine hydrate / Pd/C / ethanol / 2 h / Heating View Scheme
参考文献
Dunn
Organic Preparations and Procedures International, 1998 , vol. 30, # 6 p. 709 - 713
反应条件
1: 71 percent / 1 h / Heating 2: 70 percent / CaCO3, hydrazine hydrate / Pd/C / ethanol / 2 h / Heating View Scheme
参考文献
Dunn
Organic Preparations and Procedures International, 1998 , vol. 30, # 6 p. 709 - 713
反应条件
1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene / 1,4-dioxane / 2 h / 90 °C / |Inert atmosphere; |Microwave irradiation 2: hydrogen; palladium 10 on activated carbon / methanol / 16 h / 20 °C View Scheme
参考文献
SAMUMED, LLC; HOOD, John; KC, Sunil Kumar
Patent: WO2013/40215 A1, 2013 ;
参考文献
Dunn
Organic Preparations and Procedures International, 1998 , vol. 30, # 6 p. 709 - 713
