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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘吡啶
合成路线
（共 233 条）
5029-67-4
2-碘吡啶
+
86-74-8
咔唑
→
反应条件
23866-67-3
反应条件
18-crown-6 ether; copper; potassium carbonate in dichlorobenzene, o- 10 h; Heating / reflux;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2004/230061 A1, 2004 ;
Location in patent: Page/Page column 9 ;
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
反应条件
1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2: palladium diacetate; copper(II) bis(trifluoromethanesulfonate); silver(l) oxide / toluene / 24 h / 120 °C 3: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
+
1256380-82-1
反应条件
1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / tert-butyl alcohol / 48 h / 130 - 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
+
1352932-75-2
反应条件
1.1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -42 °C / Inert atmosphere 2.2: 0.5 h / Inert atmosphere 3.1: palladium diacetate / dichloromethane / 4 h / 65 - 70 °C 3.2: 4 h / 110 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
+
1256380-82-1
+
1352932-73-0
+
1352932-75-2
反应条件
1.1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -42 °C / Inert atmosphere 2.2: 0.5 h / Inert atmosphere 3.1: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / 1,4-dioxane / 48 h / 130 - 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
5029-67-4
2-碘吡啶
+
64-10-8
苯基脲
→
反应条件
2327-17-5
1-苯基-3-吡啶-2-基脲
反应条件
copper(I) oxide; potassium tert-butylate in 1-methyl-pyrrolidin-2-one T=100°C; 0.333333 h; Inert atmosphereMicrowave irradiation;
参考文献
Gavade, Sandip N.; Balaskar, Ravi S.; Mane, Madhav S.; Pabrekar, Pramod N.; Shingare, Murlidhar S.; Mane, Dhananjay V.
Chinese Chemical Letters, 2011 , vol. 22, # 3 p. 292 - 295
5029-67-4
2-碘吡啶
+
615-43-0
2-碘苯胺
→
反应条件
245-47-6
(7CI,8CI,9CI)-吡啶并[1,2-a]苯并咪唑
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in anhydrous xylene T=120°C; Ullmann type reaction; 12 h; Inert atmosphere;
参考文献
Wu, Zhiqing; Huang, Qing; Zhou, Xiangge; Yu, Lintao; Li, Zhengkai; Wu, Di
European Journal of Organic Chemistry, 2011 , # 27 p. 5242 - 5245
5029-67-4
2-碘吡啶
+
615-36-1
2-溴苯胺
→
反应条件
245-47-6
(7CI,8CI,9CI)-吡啶并[1,2-a]苯并咪唑
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in anhydrous xylene T=120°C; Ullmann type reaction; 24 h; Inert atmosphere;
参考文献
Wu, Zhiqing; Huang, Qing; Zhou, Xiangge; Yu, Lintao; Li, Zhengkai; Wu, Di
European Journal of Organic Chemistry, 2011 , # 27 p. 5242 - 5245
5029-67-4
2-碘吡啶
→
反应条件
2294-75-9
反应条件
1.1: pyridine-2-carboxylic acid; copper(l) iodide; caesium carbonate / 1,4-dioxane / 16 h / 70 °C / Inert atmosphere 2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 25 °C 3.1: sodium hydroxide / methanol / 16 h / 25 °C 3.2: pH 4 4.1: citric acid / methanol / 60 °C / pH 4 4.2: 25 °C / pH 12 View Scheme
参考文献
Donald, Craig; Boyd, Scott
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3853 - 3856
5029-67-4
2-碘吡啶
+
1003-98-1
2-溴-4-氟苯胺
→
反应条件
136343-75-4
(9CI)-8-氟吡啶并[1,2-a]苯并咪唑
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in anhydrous xylene T=120°C; Ullmann type reaction; 24 h; Inert atmosphere;
参考文献
Wu, Zhiqing; Huang, Qing; Zhou, Xiangge; Yu, Lintao; Li, Zhengkai; Wu, Di
European Journal of Organic Chemistry, 2011 , # 27 p. 5242 - 5245
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