3-羟基-3-甲基谷氨酸合成路线 （共 56 条）
反应条件
1: 60 percent / K2CO3, Katamin AB / acetone / 3 h / 40 - 45 °C 2: 76 percent / NaNO2, 50percent nitric acid / 5 h / 35 - 40 °C View Scheme
参考文献
Sargsyan, M. S.; Manukyan, A. T.; Mkrtumyan, S. A.; Gevorkyan, A. A.
Chemistry of Natural Compounds, 1990 , vol. 26, # 1 p. 24 - 25
Khimiya Prirodnykh Soedinenii, 1990 , # 1 p. 31 - 32
参考文献
Sargsyan, M. S.; Mkrtumyan, S. A.; Gevorkyan, A. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 10 p. 1963 - 1967
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2220 - 2224
反应条件
sodium hydroxide; dihydrogen peroxide Yield given. Multistep reaction;
参考文献
Yavrouian, Andre H.; Sanchez, Robert A.; Pollard, John K.; Metzner, E. Kurt
Synthesis, 1981 , # 10 p. 791 - 793
反应条件
sodium hydroxide 2 h; Ambient temperature;
参考文献
Mimaki, Yoshihiro; Sashida, Yutaka
Phytochemistry (Elsevier), 1990 , vol. 29, p. 2267 - 2271
反应条件
sulfuric acid; dihydrogen peroxide; acetic acid
参考文献
Eggerer; Lynen
Justus Liebigs Annalen der Chemie, 1957 , vol. 608, p. 71,77
反应条件
nitric acid 1. adding, 7 h; 50-60 deg C, 1 h;
参考文献
Devekki, A. B.; Egor'kov, A. N.; Blanshtein, I. B.; Devekki, A. V.; Idlis, G. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 9 p. 1066
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 9 p. 1284
反应条件
potassium hydroxide 24 h; Ambient temperature;
参考文献
Fujioka, Toshihiro; Masayo, Iwamoto; Iwase, Yukiko; Hachiyama, Shizuko; Okabe, Hikaru; et. al
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 7 p. 1770 - 1775
反应条件
potassium hydroxide 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Fujioka, Toshihiro; Masayo, Iwamoto; Iwase, Yukiko; Hachiyama, Shizuko; Okabe, Hikaru; et. al
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 7 p. 1770 - 1775
反应条件
potassium hydroxide 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Fujioka, Toshihiro; Iwamoto, Masayo; Iwase, Yukiko; Hachiyama, Shizuko; Okabe, Hikaru; et al.
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 9 p. 2355 - 2360
反应条件
potassium hydroxide 24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Fujioka, Toshihiro; Iwamoto, Masayo; Iwase, Yukiko; Hachiyama, Shizuko; Okabe, Hikaru; et al.
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 9 p. 2355 - 2360
