1-氯-3-甲基-2-丁烯合成路线 (共 287 条)
反应条件
Zn/Gr
5 h; Ambient temperature;
参考文献
Marceau, P.; Gautreau, L.; Beguin, F.; Guillaumet, G.
Journal of Organometallic Chemistry, 1991 , vol. 403, # 1.2 p. 21 - 27
反应条件
chromium dichloride in tetrahydrofuran
T=55°C; Hiyama-Nozaki reaction; 3 h;
参考文献
Schrekker, Henri S.; De Bolster, Martin W. G.; Orru, Romano V. A.; Wessjohann, Ludger A.
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 1975 - 1981
反应条件
(i) Mg, Et2O, (ii) /BRN= 907359/, (iii) H2, Pd-C; Multistep reaction;
参考文献
Lion,C.; Dubois,J.-E.
Bulletin de la Societe Chimique de France, 1976 , p. 1875 - 1878
反应条件
1: dimethylformamide
View Scheme
参考文献
Charreau, Philippe; Julia, Marc; Verpeaux, Jean-Noel
Journal of Organometallic Chemistry, 1989 , vol. 379, p. 201 - 210
反应条件
1.) K in diethyl ether
24 h; Ambient temperature;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, Christian
Journal of Organometallic Chemistry, 1988 , vol. 344, p. 9 - 28
反应条件
1: (i) Mg, Et2O, (ii) /BRN= 878156/
2: (i) Cu2Br2, Et2O, (ii) /BRN= 1732380/, (iii) /BRN= 1900390/
View Scheme
参考文献
Chuit; Cahiez; Normant; Villieras
Tetrahedron, 1976 , vol. 32, # 14 p. 1675 - 1680
反应条件
(i) dioxane, Et2O, (ii) /BRN= 3660023/, (iii) /BRN= 1900390/; Multistep reaction;
参考文献
Chuit; Cahiez; Normant; Villieras
Tetrahedron, 1976 , vol. 32, # 14 p. 1675 - 1680
反应条件
1: (i) NaH, (ii) /BRN= 878156/
2: BF3-Et2O
3: aq. NaOH
4: NaNH2
5: NiCl2*6H2O, NaBH4
View Scheme
参考文献
Dilbeck; Field; Gallo; Gargiulo
Journal of Organic Chemistry, 1978 , vol. 43, # 24 p. 4593 - 4596
反应条件
in tetrahydrofuran
T=30°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Kajihara, Yasushi; Ishikawa, Katsuhiro; Yasuda, Hajime; Nakamura, Akira
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 10 p. 3035 - 3036
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=0°C; 10 h;
参考文献
Kajihara, Yasushi; Ishikawa, Katsuhiro; Yasuda, Hajime; Nakamura, Akira
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 10 p. 3035 - 3036