1-萘-1-基-3-苯基-脲合成路线 (共 6 条)
反应条件
potassium phosphate; copper(l) iodide; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide
T=85°C; 24 h;
参考文献
Gavade, Sandip N.; Balaskar, Ravi S.; Mane, Madhav S.; Pabrekar, Pramod N.; Shingare, Murlidhar S.; Mane, Dhananjay V.
Chinese Chemical Letters, 2011 , vol. 22, # 6 p. 675 - 678
反应条件
copper acetylacetonate; potassium tert-butylate in 1-methyl-pyrrolidin-2-one
T=20°C; 24 h; Inert atmosphereSealed vial;
参考文献
Gavade, Sandip; Balaskar, Ravi; Mane, Madhav; Pabrekar, Pramod N.; Mane, Dhananjay
Synthetic Communications, 2012 , vol. 42, # 11 p. 1704 - 1714
反应条件
in 1,4-dioxane
T=100 - 110°C; 7 h; Inert atmosphere;
参考文献
Hosseinzadeh, Rahman; Sarrafi, Yaghoub; Aghili, Nora
Chinese Chemical Letters, 2010 , vol. 21, # 10 p. 1171 - 1174
反应条件
in tetrahydrofuran
T=20°C; 17 h; Inert atmosphere;
参考文献
Kadam, Sandip A.; Haav, Kristjan; Toom, Lauri; Haljasorg, Toiv; Leito, Ivo
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2501 - 2513
反应条件
1: benzene
2: Hydrolysis
View Scheme
参考文献
Senier; Shepheard
Journal of the Chemical Society, 1909 , vol. 95, p. 504
参考文献
Dixon
Journal of the Chemical Society, 1901 , vol. 79, p. 104