二(五氟苯基)亚膦基氯化物合成路线 （共 21 条）
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
反应条件
pyridine in diethyl ether
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
反应条件
pyridine in diethyl ether
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
反应条件
pyridine in diethyl ether
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
反应条件
in diethyl ether byproducts: HCl; in presence of a HCl-trap;
参考文献
Zeitschrift fuer Naturforschung, , vol. 21b, p. 920 - 923
反应条件
1: With magnesium in diethyl ether
1 h;
2: With phosphorus trichoride in diethyl ether
1 h;
参考文献
Mancino, Gaetano; Ferguson, Andrew J.; Beeby, Andrew; Long, Nicholas J.; Jones, Tim S.
Journal of the American Chemical Society, 2005 , vol. 127, # 2 p. 524 - 525
反应条件
hydrogenchloride in cyclohexane
T=20°C; Substitution; 0.333333 h;
参考文献
RajanBabu; Radetich, Branko; You, Kamfia K.; Ayers, Timothy A.; Casalnuovo, Albert L.; Calabrese, Joseph C.
Journal of Organic Chemistry, 1999 , vol. 64, # 10 p. 3429 - 3447
反应条件
1: PBr3
2: NEt4Cl
View Scheme
参考文献
Ali, Rusmidah; Dillon, Keith B.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , # 8 p. 2593 - 2596
反应条件
in diethyl ether
dropwise addn. of C6F5MgBr soln. into a cooled and mixed PCl3 soln.; N2 atmosphere; molar ratio: 2:1;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
反应条件
molar ratio of C6F5MgBr to PCl3: 1:1;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.10, page 123 - 137
