4-氯-3-甲酰基香豆素合成路线 （共 21 条）
反应条件
in ethanol T=20°C; 0.25 h; ultrasound irradiation;
参考文献
Prasad, J. Venkata; Reddy, J. Satyanarayana; Kumar, N. Ravi; Solomon, K. Anand; Gopikrishna
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 673 - 679
参考文献
Wu, Jie; Wang, Xiaocong
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 7 p. 1348 - 1351
反应条件
water; sodium hydrogencarbonate Heating;
参考文献
Milevskii; Chibisova; Solov'Eva; Anisimova; Lebedev; Ivanov; Traven
Chemistry of Heterocyclic Compounds, 2013 , vol. 48, # 12 p. 1781 - 1792
Khim. Geterotsikl. Soedin., 2013 , vol. 48, # 12 p. 1903 - 1915,13
反应条件
in ethanol T=20°C; 0.25 h; ultrasound irradiation;
参考文献
Prasad, J. Venkata; Reddy, J. Satyanarayana; Kumar, N. Ravi; Solomon, K. Anand; Gopikrishna
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 673 - 679
反应条件
1: 93 percent Spectr. / CHCl3 / 2 h / 20 °C 2: 8 percent / aq. AcOH / 100 °C View Scheme
参考文献
Alberola; Calvo; Gonzalez-Ortega; Encabo; Sanudo
Synthesis, 2001 , # 13 p. 1941 - 1948
反应条件
1: 80 percent / 100 °C 2: 60 percent / methanol / 2 h / 0 - 5 °C View Scheme
参考文献
Khidre, Maha Darwish
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 10 p. 2147 - 2158
反应条件
1: 80 percent / 100 °C 2: 70 percent / methanol / 2 h / 0 - 5 °C View Scheme
参考文献
Steinfuehrer, Thorsten; Hantschmann, Achim; Pietsch, Michael; Weissenfels, Manfred
Liebigs Annalen der Chemie, 1992 , # 1 p. 23 - 28
反应条件
piperidine in N,N-dimethyl-formamide
T=60 - 70°C; 2 h;
参考文献
Strakova; Petrova; Belyakov; Strakovs
Chemistry of Heterocyclic Compounds, 2007 , vol. 43, # 6 p. 793 - 798
反应条件
in methanol
T=20°C; 0.0833333 h; ultrasound irradiation;
参考文献
Prasad, J. Venkata; Reddy, J. Satyanarayana; Kumar, N. Ravi; Solomon, K. Anand; Gopikrishna
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 673 - 679
反应条件
1: N-phenylhydrazine monohydrochloride With triethylamine in ethanol
2: 4-chloro-2-oxo-2H-chromene-3-carbaldehyde in ethanol
T=15 - 25°C;
参考文献
Hamdi, Naceur; Fischmeister, Cedric; Puerta, M. Carmen; Valerga, Pedro
Medicinal Chemistry Research, 2011 , vol. 20, # 4 p. 522 - 530
